T. O. M. Microfilm Reel 027
(Original Identification Reel 27A)
Table of Contents
Note from the editors – only selected documents from this microfilm reel have been completely processed and presented below in cleaned and grouped format (Bag 2196, Sections (c), (d), and (f) only, identified by HTML links). The remainder of the reel is not related to the Fischer-Tropsch process, and therefore complete processing cannot be justified at this time.
We are, however, making the entire reel contents available in raw image format, although in a small number of relatively large files (rather than a very large number of small individual images). Anyone interested in pursuing the non-FT related material on this reel may find the document in these larger raw files.
Images 0001-0100 File size ca. 40 Mb
Images 0101-0200 File size ca. 40 Mb
Images 0201-0300 File size ca. 33 Mb
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Images 0401-0500 File size ca. 31 Mb
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Bag 2169, Target 30/4.03 – Ludwigshafen
(a) Catalyst Manufacture and Properties
1. Supply of sodium sulfide for sulfigran
2. Life of brown oxide catalyst
3. Preparation of xircon oxide gel
4. Preparation of Tonalon (Water-soluble alumina)
5. Preparation of N-catalyst for ammonia oxidation
6. Preparation of B.S. catalyst
7. Preparation of B.Z. catalyst
8. Brown oxide catalys plant for Frose
9. Sketch of B.S. and B.Z. manufacture
10. Flow sheet for B.Z. Catalyst manufacture
11. Order for rotary kiln
12. Metal requirements for Frose catalyst plan
13. Drawings of Frose Catalyst plant
14. Miscellaneous information on brown oxide catalyst manufacture at Frose and Gapel
15. Operating description of brown oxide catalyst plant
(b) Manufacture of Ethylene Glycol from Methylacetal, CO and Hydrogen
16. Inspection of Leuna Formaldehyde Plant
17. Production of Vanol
(c) H2S Absorption on Activated Charcoal
18. Cost estimate for a desulfurization plant. September 27, 1941. 3 pages.
19. Description of plant for gas desulfurization (Scholven III). July 1941. 9 pages.
20. Flow sheets of activated charcoal desulfurization. 3 pages.
21. Request for Bidon desulfurization plant. January 18, 1939. 2 pages.
22. Activated charcoal plant for Scholven. June 1, 7, and 17, 1939. 5 pages.
23. Conference and notes on desulfurization of water gas (Scholven III). June and July, 1939. 18 pages.
24. Desulfurization (Scholven III and Brux). July 7, 1939. 2 pages.
25. F- and M- Charcoal absorption, Waldenburg. September and October, 1943. 2 pages.
26. Desulfurization plant for Brux. June 29, 1939. 4 pages.
27. Desulfurization at Leuna. March 7, 1940. 2 pages.
(d) Hydrocarbon Synthesis Starting with CO and Hydrogen (Fischer-Tropsch)
28. Description of I.G. Fischer-Tropsch. By Schlecht, et al. February 16, 1943. 2 pages.
29. Cobalt Supply Situation. By Dr. Altpeter. February 16, 1943. 1 page.
30. Priority certificate for experimental CO and H2 plant. 3 pages. Very poor legibility.
31. Berlin conference on CO-H2 Synthesis. September 15, 1942. 2 pages.
32. CO + H2 synthesis with oil recirculation. January 5, 1942. 2 pages.
33. Catalyst for Hydrocarbon Synthesis. Undated. 3 pages.
(e) Difficulties with Iso-octane from Heydebreck
34. High Pour Point Difficulties with Iso-octane
35. High Pour Point Difficulties with Iso-octane
(f) Manufacture of Industrial Gases
36. Emergency measures for gas production. July 4, 1944. 9 pages.
37. Gas manufacture at Oppau. June 25, 1943. Production tables and plant flow sheets. 11 pages.
38. Condensation of water from hydrogen manufacture. By Dr. Sachsse. December 5, 1942. 24 pages.
39. Experiments on CO conversion. By Dr. Friederici. February 26, 1941. 6 pages.
41. Preparation of synthesis gas. March 18, 1941. 3 pages.
(g) Substances for Gasproofing of Textiles
43. Method for increasing the efficiency of gas proofing materials
43a. Gasproof fabrics
44. Gasproof fabrics
45. Gasproof fabrics
46. Gasproof fabrics
(h) Miscellaneous
47. Order for experimental work on the reactions of olefins with CO and H2 in the presence of sodium salt of sulfanilic acid
48. Order for experimental work on the dehydrogenation of light hydrocarbons with fixed bed catalysts
49. Order for experimental work for the preparation of synthetic fats, fatty acids and glycerine
50. Order for experimental work on the preparation of Toluene with chlormethyl and benzene
51. Preparation of water emulsions of polyisobutylene
52. Continuous production of Polyisobutylene
53. Fuming acid for artifical fog
54. Removal of artifical fog from intake to air compressors
55. Conference on analytical determination of olefins
56. Drying with silica gel
57. Experiments on the drying of liquids with silica gel
Bag 2007, Target 30/4.03 - Ludwigshafen
(a) Analytical Methods and Physical and Chemical Data
1. Definition of carbonyl and acetyl number
2. Determination of carbonyl groups in aldehydes and ketones
3. Table of vapor pressure of methylbutandiol – 1,4
4. Determination of 1,4-butanediol in crude solution
5. Heat of combustion of some nitriles, acids and esters.
6. Analysis of di-isobutylene
7. Vapor pressure of tetrahydrofuren containing water and nickel carbonyl
(b) Preparation and Utilization of Pimelic Acid
8. Use of the hexamethylenediamine salt of pimelic acid for the manufacture of bristles
9. Use of pimelic acid in the manufacture of polyamides
10. Use of pimelic acid in the manufacture of polymides
11. Ethylhexanol esters of pimelic and related acids as
12. Process for the manufacture of pimelic acid
13. Preliminary economic balance of pimelic acid manufacture
(c) Explosion Experiments on Acetylene and its Derivatives
14. Explosion experiments on mono- and divinylacetylene
15. Effect if tube diameter and wall thickness on the propagation of a detonation wave
16. Explosion experiments on acetylene
(d) Problems of the Butadiene Manufacture
17. Continuous distillation plant at Schkopau
18. Removal of SiO2 from crude butynediol solution
(e) Manufacture and Utilization of Propargyl Alcohol
19. Rust remover PL (Propargyl-alcohol – HC1)
20. Plant distillation of propargylalcohol
21. Effect of aqueous propargyl alcohol containing formic acid on iron
22. Flow sheet for separation of propargyl alcohol from formaldehyde by distillation
23. Proposed mathod of manufacture of allylalcohol from propargyl alcohol
(f) Chemical Engineering Investigations
24. Investigations on bubble plate designs
25. Investigations on driers
26. Investigations on filters
27. Various investigations on chemical engineering apparatus
(g) Preparation of Organic Chemicals
28. Patent application on the preparation of derivatives of –3 tetrahydrobenzoic acid
29. Patent application on the preparation of salts of hydroxycarboxylic acids
30. Recycle butadiene from the Buna Polymerization as basis for new manufacturing processes
31. Patent application on the preparation of diol derivatives
32. Part of patent application on the preparation of nitriles
33. Patent application on the manufacture of carboxylic acids
34. Patent application on the manufacture of carboxylic acids
(h) Drawings on Manufacture of Chemicals for Synthetic Rubber
Drawing No. Title
35. L-15175a-2 Tetrahydrofuran Distillation
36. L-6119b-1 Tetrahydrofuran Reactors
37. L-6120b-1 Tetrahydrofuran Reactors
38. L-15606a-2 Alkylation
39. L-15607a-2 Alkylation
40. L-6083a-2 Benzene-Ethylbenzene Distillation
41. L-5884a-1 Ethyl Benzene Dehydrogenation
42. L-4225c-1 Styrene Distillation
43. L-14407b-2 Styrene Distillation
44. L-15715-2 Material Balance
45. L-5202a-1 Apparatus
46. An19a Flowsheet
47. L-5707 Apparatus & Piping
48. L-5204a-1 Building
49. L-13471f-2 Flowsheet – one reactor cell
50. L-5769d-1 Reaction chamber
51. L-4118a-1 Degasification column
52. L-5167e-1 Degasification Flowsheet
53. L-5481e-1 Acetylene Pumps
54. L-5861e- Piping-Elmo chamber
55. L-6328b-8 Flowsheet-acetylene residue gas wash
56. Lu-128 Material Balance
57. IN 22e Flow Diagram
58. In 25a Detail flowsheet
59. L-5201d-1 Flowsheet
60. L-5675f-1 Tankage
61. SK 2/1/45 New Flowsheet
62. - - - New plot plan
63. L-13532b-2 Plot plan
64. L-5167C-1 Degasification
65. L-5942a-1 Flowsheet
66. L-5943a-1 Reactors
67. L-5944a-1 Distillation
68. L-5052b-1 Piping
69. N-12280C-2 Flowsheet (proposal)
End of Reel 027.