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High Efficiency Desulfurization of Synthesis Gas:
September 2000 - August 2001 Annual Report

Mukherjee, Anirban
Yi, Kwang-Bok
Podlaha, Elizabeth J.
Harrison, Douglas P.

Louisiana State University

In the pdf format this document has 36 pages and is 2.2MB.

Table of Contents

Disclaimer

i

Abstract

ii

Table of Contents

iii

List of Figures

iv

List of Tables

v

Executive Summary

vi

1

Introduction

1

 

1.1

High Temperature Gas Desulfurization

1

1.2

Ceria-Zirconia Catalyst Research

3

2

Electrochemical Synthesis and Characterization of Ce1-xZrxO2

4

 

2.1

Electrochemical Experimental

4

2.2

Solid State Analyses

5

2.3

Electrosynthesis Results and Discussion

6

 

2.3.1

Compositional

6

2.3.2

XRD and TEM Characterization

7

2.3.3

Electrochemical Process Characterization

12

3

High Temperature Desulfurization

16

 

3.1

Fixed-Bed Reactor

16

3.2

Gas Analysis

18

3.3

Materials

20

3.4

Preliminary Results

23

4

Conclusions

26

5

References

27