Determination of Solid and Liquid Impurities in Synthesis Gas - 1954
L. J. Kane1/
H. W. Wainwright1/
C. C. Shale2/
A. E. Sands3/
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| Section
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Summary and conclusions | 1 | |
| Introduction | 1 | ||
| Acknowledgments | 2 | ||
| Sampling the gas stream | 3 | ||
| Laboratory-scale equipment for testing sampling methods | 3 | ||
| Procedure | 3 | ||
| Selection of sampling point | 3 | ||
| Sampling methods | 5 | ||
| Section
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Sampling in pilot plants | 6 | |
| High temperature sampling | 7 | ||
| Separation of the solid and liquid impurities from the sample gas stream | 8 | ||
| Crude gas | 9 | ||
| Filters | 9 | ||
| Section
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Highly purified gas | 12 | |
| Large-area filter papers | 13 | ||
| Designs for large-area filter-paper holders | 14 | ||
| Gas under superatmospheric pressures | 14 | ||
| Examination of the solid and liquid impurities | 15 | ||
| Weighing procedure | 15 | ||
| Weighing large-area filters | 17 | ||
| Use of automatic instruments | 17 | ||
| Moisture determination | 17 | ||
| Particle-size determination | 18 | ||
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4 730kb |
Dispersion | 19 | |
| Section
5 730kb |
Particle-size measurement | 21 | |
| Microscopic examination | 23 | ||
| Petrographic methods | 23 | ||
1/ Chemical engineer, Synthesis Gas Branch, Bureau of Mines, Morgantown, W. Va.
2/ Chemist, Synthesis Gas Branch, Bureau of Mines, Morgantown, W. A.
3/ Assistant chief, Synthesis Gas Branch, Bureau of Mines, Morgantown, W. Va.; now with Carbide and Carbon Chemicals Corp., Oak Ridge, Tenn.