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T.O.M. Microfilm Reel 279

(Original Designation Reel BM 52)

Table of Contents

Note from the editors - only selected documents from this microfilm reel have been completely processed and presented below in cleaned and grouped format (identified by HTML link below).  The remainder of the reel is not related to the Fischer-Tropsch process, and therefore complete processing cannot be justified at this time.

We are, however, making the entire reel contents available in raw image format, although in a small number of relatively large files (rather than a very large number of small individual images).  Anyone interested in pursuing the non-FT related material on this reel may find the document in these larger raw files. 

Images 0001-0200                 File size ca.  67 Mb

Images 0201-0400                 File size ca.  61 Mb

Images 0401-0600                 File size ca.  65 Mb

Images 0601-0668                 File size ca.  22 Mb

Images 0736-0804                 File size ca.  20 Mb

Bureau of Mines Translations:  (T-461, T-471, T-477, T-481, T-483, K-1. K-2 not included).

T-460      Totzek.  Reply of Mr. Totzek of the Heinrichs Koppers Company of Essen, Germany, to a letter by the North   German Coal Control, May 2, 1947.  Translation of a document found on TOM Reel 238, Part A.  Frames 0001-0008

T-462      Latest German Developments on the Gas Phase.  Gasoline Synthesis at Middle Pressures, 1942-1945.  By Dr. Ackermann.  PB 82,060.  Translation of a document found on Fiat Reel X-116 (TOM reel 305), Frames 1717-1787.  Frames 0009-0018.  10 pages.

T-463      Three papers on the Duftschmid Oil Circulation Process. I.  July 25, 1941.  4 pp. II. Brief Report on the Hydrocarbon Synthesis from Carbon Monoxide and Hydrogen by the Oil Circulation Process.  Oct. 9, 1939.  3 pp. III.  State of Experiments on Alcohol Synthesis by the Oil Circulation Porcess.  August 11, 1941.  11 pp.  By Duftschmid.  Translation of documents found on TOM Reel 134, Items I(b) 11; I(b) 12; I(b) 13.  Frames 0019-0035.  17 pages.

T-464      The Status of Hydrocarbon Synthesis from CO-H2 Mixtures.  By Dr. Michael.  July 24, 1941.  Translation of a   Document found on TOM Reel 164, Frames 143-153.    Frames 0036-0048

T-465      Boente.  Solid Aromatics in the HOLD of Pitch Hydrogenation, Poelitza.  July 15, 941.  Translation of a document found on TOM Reel 164, Frames 190-192.  Frames 0049-0051

T-466      Koppers-Totzek Powderd Coal Gasification,  (A paper read by Friedrich Totzek, July 2, 1947, in Essen).   Umschau, Vol. 66/67, p. 363.  Frames 0052-0056.  5 pages.

T-467      Frese.  Hydrogenation of Bituminous Coal LTC Pitch.  (From Dr. E. L. Frese’s files, Main Laboratory,   Ruhrol G.m.b.H., Bottrop).  Dec. 1944.  Frames 0057-0105

T-468     Hydrocarbon Synthesis with an Iron Catalyst.  By Kolbel.  Sept. 13, 1940.  Translation of a document found on TOM Reel 178, Frames 2627-2642.  Frames 0106-0126.  21 pages.

T-469     Hydrocarbon Synthesis with Iron Catalysts.  By Dr. Roelen.  Ruhrchemie A.G., Sept. 13, 1940.  Translation of a document which appears on TOM Reel 178, Frames 2643-2669.  Frames 0127-0147.  21 pages.

T-470      Three papers by Otto.  I.  Operating Directions for Starting the Producer.  Nov. 7, 1941.  6 pp.  II.  Operating Directions for the Producer Plant: Boehlen, Feb. 7, 1942.  10 pp.  III. Operations for Stopping the Gasifiers, Second Edition.  Boehlen, Aug. 30, 1943.  8 pp. incl. 2 graphs.  Translation of documents which appear on TOM Reel 12, Item 33.  Frames 0148-0171.  24 pages.

T-472      Donath, Dr. E.E. Calculation of Hydrogenation of Naphthenes.  July 27, 1938.  High Pressure Experiments, Ludwigshafen 558.  Frames 0172-0179

T-473      Gunther.  Refining of Liquid Phase Gasoline from Scholven.  March 25, 1942.  High Pressure Experiments.  Ludwigshafen.  Frame 0180

T-474      Three papers on the Aromatics-Naphthenes Equilibrium.  I.  Aromatics-Naphthenes Equilibria Curves.  May 22, 1943.  Peters II.  The Production of Aromatics-Naphthenes Equilibria on the Nickel-Tungsten Catalyst 6718.  Feb. 1940. 5 pp. and 4 Curves.  Peteres.  III.  The Aromatics-Naphthenes Equilibrium on the Tungsten Sulfide Catalyst 5058.  May 25m 1943.  1 p. and 1 curve.  Peters and Trofimow.  Translation of documents which appear on TOM Reel 173, Frames 699-702.  Frames 0181-0192

T-475      Brief summaries of three papers on Splitting Hydrogenation.  I.  Splitting Hydrogenation Catalyst with HF Treated Alumina as Carriers.  June 12, 1941.  Rotter.  Document appears on TOM Reel 173, Frames 483-488.  II.  Tungsten-Free Splitting Catalyst of the SiO2-AL2O3-Fe2O3 Mixtures Treated with HF.  May 1944.  Gunther,  Document appears on TOM Reel 173, Frames 401-408.  III. The Splitting Hydrogenation of DHD Residues.  Feb. 1, 1943.  Gieg and Simon.  Document appears on TOM Reel 173, Frames 366-392.  Frames 0193-0199

T-476      Peters and Gunther.  Upper Limits of N and Phenol Contents and Lower Limits for the Aniline Point of 6434. Injection.  Dec. 17, 1940.  Translation of a document which appears on TOM Reel 173, Frames 642-644.  Frames 0200-0202

T-478      Connection between Nitrogen Content of Oils and their Splitting Hydrogenation Ability (Splitability).  Three papers by Gunther, dated March 23, 1942, Jan. 8, 1943, July 13, 1943.  Translation of documents appearing on TOM Reel 173, Frames 633-641, 621-628, and 565-567.  Frames 0203-0227

T-479      Gunther, Hartmann and Simon.  Replacing of Terrana in 6434 by Synthetic Silicates.  Sept. 21, 1939.  Translation of a document appearing on TOM Reel 173, Frames 549-553.  Frames 0228-0230

T-480      Peters and Gunther.  Terrana-Zinc Sulfide-Tungsten and Terrana-Zinc Sulfide-Molybdenum Catalysts for Splitting Hydrogenation.  Dec. 11, 1939.  Translation of a document which appears on TOM Reel 173, Frames 541-548.  Frames 0231-0235

T-482      Composition and Preparation of 6434 Catalyst.  May 10, 1944.  Translation of a document which appears on TOM Reel 173, Frame 409.  Frames 0236-0237

T-484      Refining Catalysts 7525, 7675, 7360, 7846.  Nov. 1940.  Translation of a document which appears on TOM Reel 173, Frames 198-199.  Frames 0238-0239

T-485      Gunther.  Prehydrogenation Catalysts.  The Use of 8676 Prehydrogenation Catalyst (Alumina-W-Ni) for Various Feeds.  Oct. 1942.  Translation of a document which appears on TOM Reel 173, Frames 320-328.  Frames 0240-0241

K-3          Pier, M. Hydrogenation Gasolines.  Effect of Raw Materials, Catalysts, and Operating Procedures.  Taken from Angewandte Chemie, Vol. 51 (1938), pp. 603-608.  Frames 0242-0265

K-4          Thibaut, Louis.  Development of the Technique of Hydrogenation of Solid Fuels and of Their By-Products.  (Paper presented by M. Thibaut, Director of the Compagnie Francaise des Essences Synthetiques, at the XX Congress of Industrial Chemistry, Paris, Sept. 22-28, 1946).  Chimie et Industrie, Vol. 59 (1948), pp.  548-551.  Frames 0266-0279

K-5          Naumann, Friederich Karl.  The Effect of Highly Compressed Hydrogen Upon Unalloyed Steel.  Translation of an article appearing in Stahl und Eisen, Vol. 57, 1937, pp. 889-899.  Frames 0280-0318

K-6          Naumann, F.K.  The Effect on Alloying Additions on the resistance of Steel to Hydrogen under High Pressure.  Translation of an article appearing in Stahl und Eisen, Vol. 58, 1938, pp. 1239-1250.  Frames 0319-0363

2              Sinclair Refining Company Translations:

SR-4        Translation Book 208.  Cracking of Shale Tars with Aluminum Chloride.  By N. I. Zelenin and N.N. Kosheleva.  Translation of a document on TOM Reel 55, Combustible Shales, No. 3 (1934), pp. 35-41.  Frames 0364-0374

SR-5        Translation Book 211.  Cracking and Hydrogenation of Esthonian and Kashpirian shales tars.  N.D. Tilicheyev and G.N. Sledzhiev.  Translation of a document found on TOM Reel 255, Chemistry of Solid Fuels, Vol. 2, No. 2 (1931), pp. 3-15.  (Sinclair translated only part of the article.)  Frames 0375-0384

SR-6        Translation Book 210.  Thermal Decomposition of Gdov Shales under Hydrogen Pressure.  By V.P. Tsybasov, S.A. Dymshits and I.S. Levit.  Translation of a document found on TOM Reel 255, Combustible Shales, No. 4 (1935), pp. 82-87.  Frames 0385-0394

SR-7        Translation Book 212.  Preparation of Octyl Acetate and of Acetic Esters of Secondary Alcohols with More then Eight Carbon Atoms.  Translation from a document found on TON-Reel 72, Item 78.  Frames 0395-0417

SR-8        Translation Book 216.  The Interaction of the Sulfonic-Acid Chlorides, Formed by Means of Sulfochlorinating Aliphatic Hydrocarbons with Ammonia and Ammonia Derivatives.  By Dr. Asinger, Dr. Ebeneder, Dr. Boeck, Dr. Schmidt found on TOM Reel 221, Bag 3045, Item 25, Frames 250000451-484.  Frames 0418-0439

SR-9        Translation Book 219.  The Constitution of the Mepasin Sulfonates.  Br Dr. Asinger.  Oct. 29, 1941.  Translation of a document found on TOM Reel 21, Frames 240000438-240000450.  Frames 0440-0450

SR-10     Translation Book 222.  Preparation Character and Capillary-Chemical Properties of Hexadecane Sulfonates and Sulfates.  By Drs. Asinger, Eckhardt, and Ebeneder.  Translation of a document found on TOM Reel 21, Bag 3045, Item 26, Frames 260000485-504.  Frames 0451-0463

SR-11     Translation Book 223.  Staplization and Refining of Shale-Tar Benzine by Hydrogenation.  By A.D. Petros, E.A. Rozhiltzeba, and D.N. Andreyev.  Translation of a document found on TOM Reel 255, Chemistry of Solid Fuels, Vol. IV, No. 5, (1933), pp. 459-469.  Frames 0464-0474

SR-12      Translation Book 244.  Determination of the Hydrocarbon Groups in Shale Benzine.  By V.V. Chelintsev and A.P. Sibertsev.  Translation of a document found on TOM Reel 255, Chemistry of Soild Fuels, Vol. 4, No. 6 (1933), pp. 573-577.  Frames 0475-0481

SR-13      Translation Book 226.  Destructive Hydrogenation of Kashpir Tar.  By S.S. Nametkin, F.I. Sanin and E.F. Rudakoba.  Translation of a document found on TOM Reel 255, Chemistry of Solid Fuels, Vol. IV, No. 6 (1933), pp. 598-605.  Frames 0482-0490

SR-14      Translation Book No. 228.  Catalytic Desulfurization of Kashpir Tar Shale Benzines in the Presence of Hydrogen Under Atmospheric Pressure.  By A.S. Broun.  Translation of a document found on TOM Reel 255, Chemistry of Solid Fuels, Vol. 5, No. 3 (1934), pp. 267-273.  Frames 0491-0497

SR-15      Translation Book No. 229.  Desulfurization of Shale Benzines by Hydrogenation in the Presence of Catalysts.  By Nametkin, S.S., Senin, P.I., Makover, S.B. and Tzibe, A.N.  Translation of a document found on TOM Reel 255, Chemistry of Solid Fuels, Vol. 5, No. 4 (1934), pp. 333-357.  Frames o498-0525

SR-16      Translation Book 241.  Hydrogenation of the Neutral Kerosene Fraction of Gdov Shale Tar.  By Klukvin, N.A., Polozov, R. Ph., and Pheophilov, E.E.  Translation of a document found on TOM Reel 255, Chemistry of Solid Fuels, Vol. 6, No. 4 (1935), pp. 340-347.  Frames o526-0535

SR-17     Translation Book 242.  Phenols from Primary Tars and their Stabilizing Influence upon Shale Benzines in Comparision with Synthetic Inhibitors.  By N.V. Ershov. Translation of a document found on TOM Reel 255, Journal of Applied Chemistry (USSR), Vol. XII, No. 6 (1939), pp. 875-877.  Frames o536-0539

Translation Book 169.  Detailed Discussion of Meiler Operation on Oil Shale at Balingen.  (Building Project).

Translation of a document found on TOM Reel 123, frames 85-121.  Frames 0540-0550

Translation Book 174. Dewaing of Crude Oil with Solvents in the Liquid Phase for the production of Cold Resistant Oils.  Report by Dr. J. Moos.  Translation of a document found on TOM Reel 113, Document 10m Item 1.  Frames 0551-0580

Translation Book 176.  The Refining of Petroleum and Lignite-Tar Fractions with Liquid Hydrofluoric acid to Produce Diesel-Fuel, Lubricants and Fuel oil for the Armed Forces.  Federal Institute for Petroleum Research, Institute for Technology, Hannover, July 7, 1944.  Translation of a document found on TOM Reel 113, Item 6.  Frames 0581-0601

Translation Book 196.  Flow Sheet.  Preparation of HF Catalyst.  Translation of a document found on TOM Reel 195, Part 12, Doc. 9, Frame 31504.  Frames 0602-0604

3.             Detection of Iso- and Alicyclic Compounds in Saturated Hydrocarbon Mixtures.  By Dr. Dornow. Petroleum Institute of Hanover Technical School, July 7, 1944.  (Translation by Standard Oil Development Co., from a document found on TOM Reel 73, Item 5, Frames 587-607.    Frames 0605-0610

4.             Refining of Light Oil from Low Temperature Carbonization of Coal.  By W. H. Oppelt.  Frames 0611-0619

5.             Azienda Carboni Italiani.  Description of the plant.  (Translation of an Italin document).  Frames 0620-0653

6.             A chronological summary of and comments on Dr. Michael’s Liquid Phase Process.  (Schaumfahrweise).  By L. W. Alberts.  Frames 0654-0662.  9 pages.

7.             Report of “Fouchers” on CO+H2 Synthesis.  (I.G. Farben), October 1947.  Section II of Part I Oil recycle Process.  Comments by L. W. Alberts.  Frames 0663-0666.  4 pages.

8.             Report for the FIAT consisting of a letter and drawing by Dr. Winkler on the subject of “Vergasung von feiner kohle nach dem Verfahren von Dr. Winkler”.  (Carburation of coal dust accordIng to the Winkler Process).  Frames 0667-0668.  2 pages.

9.             Report by Dr. Fr. Winkler entitled:  “Historische Entwicklung der Vergasung von feinkornigen Kohlennach dem Verfahren con Fritz Winkler.” (Historical Development of the Gasification of Fine Coal according to a Process Developed by Fr. Winkler.)  Part I.  Frames 0669-0720.  52 pages.  In German.

10.           Report by F. Halle, L. Lorenze and G. Wetzel entitled: “Rontgenographische Untersuchung der Carbidierung von Nickelpraparaten im CO-Strom zwischen 140° and 250°.”  (X-Ray Examination of the Carbidization Process of Nickel Preparations in CO Current between 140° and 250°.) Part II.  Frames 0721-0739

11.           A group of German memos relating to the above report.  Included are memos:  70, 71, 72, 73, 74, 75, 78, 84, 93, 94, 103, 104, 105 and 114.  Frames 0740-0753.

12.           The Synthesis Of CO+H2 at I.G. Farben.  Part III.  Polymer Gasolines (“La Synthese CO+H2 at I.G. Farben. 3 Partie. Les Essences de Polymerisation”).  Included in this paper are the following reports:  Frames 0754-0788

1.        “Magnesiumphosphatkentakt.”  (Magnesium phosphate catalyst.)  4 pp.  By Dr. Schutze.  7/14/47.

2.        “Versuche zur technischen Herstellung des polymerbenzinkontaktes.”  (Investigations on the technical production of polymeric gasoline catalysts,)  1 p, By Dr. Schutze. 7/14/47.

3.        “Polymerbenzinkontakt.”  (Polymeric gasoline catalyst.)  1 p.  By Dr. Rabe.  8/28/47.

4.        “Polymerisationsanlage Schwarzheide.  I. Mitteldruckanlage,  II.  Hochdruckanlage.”  (Polymerisation Installations at Schwarsheide.  I.  Middle Pressure Installation.  II.  High Pressure Installation.)  4 pp. and 1 diagr.  By Dr. haubach.  7/15/47.

5.        “Versuche zur homogen Verteilung von Phosphorsaure auf aktivierten Holzkohlen.” (Investigations on the Homogenous Distribution of Phosphoric Acid on Activated Charcoal.)  9 pp. incl. 2 tables and 1 diagr.  By Dr. Munch.  4/11/38.

6.        “Uber das Klopverhalten von Fischergas-Polymerbenzin.”  (The Knock Behavior of Fischer Gas Polymeric Gasoline.)  11 pp. Incl. 4 tables.  By Dr. Munch.  4/14/1938.

13.           Isosynthesis (“Die Isosynthese).  By Helmut Pichler and Karl-Heinz Ziesecke from the Kaiser-Wilhelm Institut fur Kohlenforschung, Mulheim.  Frames 0789-0931.  144 pages.  First 2/3’s text is good, figures awful.  Last 1/3 reversed – figures generally OK, text awful.