T.O.M. Microfilm Reel 203
(Original designation LF – 125)
Table of Contents
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Hochdruckversuche Laboratories
I. Lectures By Dr. Pier.
II. Reports On Experimental Work On Hydrogenation In The Sumpfphase. Files Of Dr. Peters.
III. Reports On Experimental Work In The Sumpf-Phase Of Dr. Peters.
Source of Documents: Griesheim Central I.G. Library
Folder Nos.: S33/I-C-9
S33/I-D-6
S33/I-D-7
Filmed by: J I O A
Date: 28 February 1946.
I. Hochdruckversuche Laboratories. Lectures by Dr. Pier. S33/I-C-9.
Item
1. Hydrogenation gasoline. Influence of crude material, catalyst and method of processing. Frames 1-34
2. Competitor Michal. Frames 35-40
3. Hydrogenation gasoline. Influence of crude material, catalyst and method of processing. Frames 41-45
4. Solid-bed catalyst and gas phase. Frames 46-54
5. Gas phase gasolines as dependant on the crude materials. Frames 55-61
6. Solid-bed catalyst and gas phase. Frames 62-69
7. Sumpf phase. Frames 70-84
8. Hydrogenation gasoline. Influence of crude material, catalyst and method of processing. Frames 85-100
9. Talk on hydrogenation delivered at Rom. Frames 101-120
10. Hydrogenation gasoline. Influence of crude material, catalyst and method of processing. Frames 121-129
11. The treatment of shale oil by hydrogenation. Frames 130-156
12. Draft for the talk on shale oil. Frames 157-162
13. Working of Scotch shale oil. Frames 163-165
14. Pressure hydrogenation experiments with Scotch shale oil. Frames 166-178
15. Lubricant from Scotch shale oil over catalysts 5058 and 6719 at different pressures. Frames 179-184
16. Talk on hydrogenation delivered at Glasgow. Frames 185-193
17. Sumpf phase. Frames 194-202
18. Gas phase. Frames 203-208
II Hochdruckversuche Laboratories. Reports on experimental work on hydrogenation in the Sumpfphase. Files of Dr. Peters – S33/I-B-6.
Item
1. Processing a pitch mixture from Welheim (P 1487 of August 18, 1941) at 600 atm to heavy oil excess in 10 litre furnace. Frames 244-272
2. Processing a mineral-coal-tar mixture for Politz at 600 arm to gasoline and heavy oil in 10 litre furnace. Frames 273- 298
3. Processing high temperature carbonization tar “Carsten Zentrum of the “Schlesag” (P 1376 from June 6, 1940) at 600 atm for excess heavy oil. Frames 299-332
4. Comparing the various “Sumpfphase” systems as to the heat required and to the course of temperature. Frames 333-336
5. Preliminary report on hydrogenation experiments with “Otto” tar and “Oheim” nutcoal. Frames 337-338
6. The accuracy of elementary uncorrected balances on the 10 liter furnace. Frame 339
7. Processing a mineral-coal-tar mixture for Politz at 600 atm for excess heavy oil in 10 liter furnace. Frames 340-372
8. Processing a mixture of coke oven tar (Ruhr) (P 1416) topped up to 325° at 600 atm, for excess heavy oil in the 10 liter furnace. Frames 373-406
9. Processing coke oven tar “Auguste Viktoria” (Ruhr) (P 1094 of July 11-39) topped up to 325° at 600 atm, for excess heavy oil in 10 liter furnace. Frames 407-437
10. Processing coke oven tar “Auguste Viktoria” (Ruhr) topped up to 325° (PM1094 of July 11-1939) at 600 atm, to gasoline and middle oil. Frames 438-476
11. Problems in processing “Rheinische Braunkohle” (soft coal). Frames 477-478
12. Preheater coils of 10 liter furnace becoming incrusted. Frames 479-485
13. Supplement: Processing of “Scholven” sludge in “Sumpf” phase at 600 atm in 1.5 liter furnace. Frames 486-489
14. Testing Brux embers as catalyst carriers. Frames 490-491
15. C-H-analyses of various products from chamber 804 Ludwigshafen charged with Upper Silesian coal for
gasoline and middle oil (August 1941). Frame 492
16. Processing Scholven coal (Zweckel coal) with iron catalyst and chlorine. Frames 493-495
17. Applying very high thru puts in processing Silesian coal for maximal excess of heavy oil. Frames 496-499
18. Processing Silesian coal “K 1174” “Castellengo – Abwehr” to gasoline and middle oil at 600 atm in 10 liter furnace. Frames 500-534
19. Experiments in 10 liter furnace on Sumpfphase problems. Frame 535
20. Processing Silesian coal “K 1180” from “Beuthengrube” for gasoline and middle oil at 600 atm in 10 liter furnace. Frames 536-582
21. The effect of the age of coal on the quality of the fuel oil. Frames 583-584
22. Processing “Scholven” sludge in Sumpfphase at 600 atm in 1.5 liter furnace. Frames 585-593
23. Experiments in processing crude oil residue from "Heide” at 600 atm to Diesel fuel. Frames 594-597
24. Note re problem of conversion of Na2CO3 to Na2S when sulfurizing the “Bayermass” with pure H2S and H2S-CO mixtures. Frame 598
25. Re: Hydrogenation of pitch. Frame 599
26. Processing Silesian Mineral coal 1160 (Preussengrube) to heavy oil excess at 600 atm in 10 liter furnace. Frames 600-630
27. Middle oil concentrations in the mineral coal “Sumpfphase” in different procedures of production. Frame 631
28. Experiments on obtaining primary bitumen for the manufacture of electrode carbon (preliminary stage). Frames 632-635
29. Experiments on heating coal paste. Frames 636-653
30. Processing Silesian coal “K 1174”. “Castellengo-Abwehr” to excess heavy oil at 600 atm in a 10 liter furnace. Frames 654-685
31. The influence of the content of middle oil in paste oil on the composition of the re-formed products when processing Silesian coal “K 1197” by varying procedures. Frames 686-691
32. Processing Silesian coal from the “Heinitz” pit to heavy oil excess under extensive decomposition of the asphalts. Frames 692-694
33. Processing hydrogenation residues rich in asphalts, by carbonizing them mixed with coal to a loose charge. Frames 695-707
34. Re: Economizing molybdenum in the Sumpfphase. Frames 708-710
35. Processing a mineral coal-tar mixture (Politz) in the 10 liter furnace over “Grude” iron-titanium catalyst. Frames 711-713
36. Composition of gases from processing Silesian mineral coal and high-temperature tar from mineral coal at 600 atm. to heavy oil. Frames 714-715
37. Processing “Boehlen” coal in the Sumpfphase. Frames 716-717
38. Experiments with mineral coal tar in the 10 liter furnace. Frames 718-719
39. Heating fuels from various mineral coals. Frames 720-724
40. Comparing the qualities of heating fuels obtained from heavy oils by various procedures. Frames 725-727
41. Program for a conference with Mr. Josenhans at Lu on January 15, 16 and 17, 1941. Frames 728-729
42. On the problem of substituting molybdenum in processing tar at Politz. Frames 730-731
43. Processing of mineral coal for various yields of heavy oil excess. Frames 732-737
44. Silesian mineral coal 1118 from the pit “Grafin Johanna” of the “Grafl. Schaffgott’schen works Ltd.”, processed for obtaining gasoline and middle oil at 600 atm. in the 10 liter furnace. Frames 738-770
45. “Sudenten” tar (“Lurgi” tar from Brux coal). Frames 771-796
46. Chlorine contents of raw material provided for “Blechhammer” and of oils produced from these. Frames 797-798
47. Processing coke oven tar pitch (admixture of chlorine). Frames 799-801
48. Hydrogenating non-de-ashed Upper Silesian coal with chlorine. Frames 802-806
49. Simultaneous hydrogenation of Silesian mineral coal and low temperature carbonization tar. Frames 807-811
50. First figures on processing high temperature tar from carbonization of Upper Silesian mineral oil. Frames 812-813
51. Status of experiments with Sudenten coal at 600 atm. Frames 814-815
52. Status of experiments with Sudenten coal at 250 atm. Frames 816-817
53. Fuel oil form stripper heavy oil. Examining stripper fractions. Frames 818-820
54. Stage of experiments with “Bubiag” coal (K 197) at 600 atm. Experiments in 1.5 liter furnace with stirrer. Frames 821-822
55. Hydrogenation of coal tar in Sumpfphase at 600 atm. to gasoline and fuel oil. Frames 823-832
56. Progress in hydrogenation of open-burning coal. Experiments with “Gelsenberg” coal (83.9% C in dry coal) in the 10 liter furnace with stirrer. Frames 833-834
III. Hochdruckversuche Laboratories. Reports on experimental work in the Sumpfphase. Files of Dr. Peters. S33/I-D-7.
Item
1. Problems of starting (in the Sumpf” phase). Evaluation of the 10 liter furnace experiments up to now. Frames 835-846
2. Processing mineral coal to gasoline, middle oil and light heavy oil. Frames 847-848
3. Centrifuging tars and sumpfphase sludges from tars. Frames 849-852
4. Sludge distillation. Report I. Frames 853-868
5. Processing “Janina” coal to gasoline and middle oil at 250 atm with iron catalysts. Frames 869-875
6. Heating fuel from “Janina” coal. Frame 876
7. Processing “Janina” coal at 600 atm to excess heavy oil. (First preliminary report.). Frames 877-879
8. Processing “Janina” coal at 600 atm to gasoline and middle oil. (Second preliminary report.). Frames 880-887
9. Relation between analyses of coal and behavior in hydrogenation. Frames 888-890
10. On pre-heating cracking residues. Frames 891-896
11. The question of incubation temperature. Frames 897-898
12. Measuring the heat transfer from mineral coal paste. Frame 899
13. Hydrogenation of “Janina” coal to gasoline and middle oil at 600 atm. First results. Frames 900-904
14. Status of experiments on the 10 liter furnace. Frame 905
15. Processing petroleum in straight passage. Frames 906-907
16. Experiments in 1-liter furnace with sulfur as “Sumpfphase” catalyst. Frames 908-913
17. “Starting” in coal hydrogenation in the Sumpfphase. Frames 914-916
18. Processing “Myslowitz” coal at 600 atm to gasoline and middle oil. Frames 917-918
19. Producing slightly hydrogenated coal from K 1197 at 300 atm. Frames 918-928
20. Comparing sodium sulfide raw smelting with Sulfigran. Frames 929-930
21. Catalyst experiments in 1.5 liter furnace for processing “Bruex” tar. Frames 931-936
22. Admixture of sodium-sulfide in mineral coal hydrogenation. Older experiments with K 1090 (Gelsenberg) in 10-liter furnace. Frames 937-964
23. Processing mineral coal together with mineral coal extract. Frames 965-966
24. Processing mineral coal high temperature tar with mineral coal admixed. Frames 967-989
25. Processing mixtures of “Bohlen” tar and petroleum (August 1939). Frames 990-1007
26. Report on experiments: Processing of Panuco-oil in 10 liter furnace. Frames 1008-1028
27. Processing “Bohlen” tar at 250 atm. in 10 liter furnace. (August 1939). Frames 1029-1043
28. Report on experiments: Processing German petroleum in 10 liter furnace. Frames 1044-1077
29. Processing mineral coal and carbonization tar to briquette binder and asphalt-free oil. Frames 1078-1121
30. Processing “Zweckelcoal” (K 1216) to gasoline and middle oil at 600 and 250 atm and to heavy oil excess at 600 atm in 10 liter furnace. Experimental report. Frames 1122-1163
31. Extractive hydrogenation of mineral coal. Frames 1164-1231
32. Processing Silesian coal (K 1197) together with Silesian mineral coal-tar mixture to a slight heavy oil excess at 600 atm in the 10 liter furnace. Frames 1232-1254
33. On “caviar” formation” Experiments with “Rhine” soft coal in 10 liter furnace. Frames 1255-1260
34. Experimental report: Processing a mixture of Silesian mineral coal tars at 600 atm to heavy oil excess in the 10 liter furnace. Frames 1261-1283
35. First figures on processing primary bitumen by hydrogenation. Frames 1284-1286
36. Re: Processing hydrogenation coal “Scholven” K 1101 of September 30, 1938, at 250 atm with chlorine, in various forms of admixture and with “Snox” for obtaining gasoline and middle oil. Report on experiments in the 10 liter furnace. Frames 1287-1330
37. Extractive hydrogenation in 10 liter furnace. Frames 1331-1335
38. Preventing crusts and blockings of coal furnaces at Scholven. Frame 1336
39. Experiments on “Caviar” formation in the rotary autoclave. Frames 1337-1338
40. Experiments with Rhine brown coal in 1 liter furnace. Note No. 3: Neutralization of coal and its tendency to deposit. Frames 1339-1340
41. Joint processing of upper Silesian coal and rinsing gas tar to briquette binding agents and to heating fuel. Frames 1341-1345
42. Experimental report: Joint processing of Silesian coal (K 1197) and high temperature carbonization tar from Silesian coal (P 1376) for obtaining slight excess heavy oil at 600 atm in 10 liter furnace. Frames 1346-1373
43. The status of experiments with Rhine brown coal. Frames 1374-1375
44. Experiments with Rhine brown coal in 1 liter furnace. Preliminary notes on “caviar” formation. Frame 1376
45. Supplement to report 20 4721 of July 16-42: Preliminary report on hydrogenation experiments with B.T. – tar from “Oheim” nut coal. Frame 1377