T.O.M. Microfilm Reel 169
(Original Designation LF-102)
Table of Contents
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Hochdruckversuche Laboratories.
I. Miscellaneous Papers On Catalysts. Files of Dr. Reichle.
II. Exchange Of Experience On Alumina. Files of Dr. Pier.
IIa. Papers On Prehydrogenation. Files of Dr. Pier.
III. Papers On Dehydrogenation. Files of Dr. Pier.
IV. Papers On Dehydrogenation. Files of Frl. Dr. Horing.
V. Papers On Dehydrogenation. Files of Frl. Dr. Horing.
VI. Papers On Hydrogenation Of Various Coals. Files of Dr. Peters.
VII. Papers On Foreign Hydrogenation Works. Files of Dr. Peters.
VIII. The Coals Of Upper Silesia. Files of Dr. Peters.
Source Documents: Griesheim Central I. G. Library
Folder Nos: S/32/VIII-D-2 S32/VIII-D-11
S/32/VIII-D-6 S33/I-D-5
S32/VII-D-6 S33/I-C-5
S32/VII-D-10 S33/I-D-6
Filmed by: JIOA
Date:
I. Hochdruckversuche Laboratories. Miscellaneous papers on catalysts. Files of Dr. Reichle.
Folder No. S32/VIII-D-2.
1. Use of alumina-W-Ni-contact 7846 W 250 – 8376 for various processes. Frames 1-2
2. Report on activity November 1941. Frames 3-15
3. Alumina-molybdenum-nickel and alumina-tungsten-nickel prehydrogenation contacts. Frames 16-21
4. Requirement of tungsten for the two stage benzination with various contact combinations. Frame 22
5. ZnO + MoO3 or ZnO + MgWO4 replacing vanadium in aromatization contact 7019. Frames 23-30
6. Conference on 3-14-41 at Lu 558 on measures for storing contacts and raw materials for contacts with regard to air raids. Frames 31-32
7. Contact 7846 for prehydrogenation of Scholven medium oil from coal liquefaction of Bruex tar (a+s-M oil) and of S-middle oil from Rhine-soft coal. Frames 33-44
8. Reduction of 7019-contact in normal operation with coal liquefaction middle oil. Frames 45-51
9. Comparing dehydrogenation contacts 7911 (Leuna) with 7360 Ch. 6 (Lu) at 10 and 25 atm and various steps of temperature (part 2). Frames 52-64
10. Notes on conference at on silica gel. Frames 65-66
11. Preliminary comparison of contact 7612/350°C with 7612 and 7360/350°C in dehydrogenation. Frames 67-69
12. Aromatization of liquefaction middle oil. Frames 70-81
13. Quality of residual gasoline in aromatizing contacts based on bleaching earth or silicates. Frames 82-84
14. Aromatizing with Weilheim contact at 600 atm. Frames 85-89
15. Causes for difference in quality of residual gasoline from aromatizing coal liquefaction products. Frames 90-99
16. Gas formation during aromatization at 250, 450 and 600 atm. Frames 100-102
17. Aromatization at 250 atm. Alumina contacts (supplement to report of 1-14-41). Frames 103-104
18. Aromatization at 250 atm. Terrana contacts. Frames 105-109
19. Aromatization at 250 atm. Compound contacts. Frames 110-112
20. Aromatization at 300 and 450 atm. Present status. Frames 113-114
21. Experiments on aromatization. Present status. Frames 115-117
22. Aromatizing benzination over 7019. Frames 118-121
23. Aromatization of 5058-B-middle oil Scholven over various catalysts. Frames 122-124
24. Aromatization of Sumpf middle oil from K 1156 (“Velsen” coal). Frames 125-130
26. Synthesis plant – Ludwigshafen. By Hubner. July 23, 1940. Frames 135-148. 16 pages.
28. Velocity and times of contact in processing bituminous coal in Sumpf phase. Frames 156-157
II. Hochdruckversuche Laboratories. Exchange of experience on alumina. Files of Dr. Pier.
Folder No. S32/VIII-D-6.
1. Exchange of experience on alumina, Oppau, 7-6-1943. Frames 158-200
IIA. Hochdruckversuche Laboratories. Papers on prehydrogenation. Files on Dr. Pier. Folder No. S32/VII-D-6.
1. Development of catalysts for prehydrogenation. Part I. up to catalyst 7745. Frames 201-208
2. Status of experiments on prehydrogenation on 8-8-40. (Improving of the Fe-W-Ni-catalyst 6719). Frames 290-217
3. Prehydrogenation over catalysts based on activated alumina. Frames 218-219
4. Report of catalyst factory on prehydrogenation-catalysts. Frames 220-221
5. Experiments on prehydrogenation with catalysts on alumina. Frames 222-223
6. The present status of experiments on prehydrogenation catalysts. Frames 224-225
7. Prehydrogenation. Frames 226-235
8. Improvement of 6719 by the addition of various components. Frames 236-241
III. Hochdruckversuche Laboratories. Papers on dehydrogenation. Files of Dr. Pier. Folder No. S32/VII-D-10.
1. DHD-gasoline endpoint 165 and 185°C. Frames 242-248
2. Dehydration and refining of polymer gasoline. Frames 249-256
3. DHD catalyst tests in 100 cc furnaces. Frames 257-266
4. DHD-catalyst tests in 100 cc furnaces. Frames 267-272
5. Processing of Hungarian gasoline to DHD gasoline. Frames 273-276
6. DHD-catalyst test in 100 cc furnaces. Frames 277-291
7. Processing of Sumpf gasoline from K 1242 to DHD-gasoline in 40 Liter Furnace 601. Frames 292-300
8. Processing of Zeitz TTH gasoline to a high power fuel by DHD method. Frames 301-309
9. Processing of gasoline from mild aromatization (contact 7501) by the DHD method. Frames 310-319
10. DHD experiments on Rumanian heavy petroleum gasoline, processed in Poelitz. Frames 320-326
11. Dehydrogenation of Rumanian heavy gasoline over powder catalyst. Frames 327-334
12. 600-atm aromatization of liquefaction middle oil as preliminary step for the preparation of DHD high power fuel. Frames 335-349
13. Utilization of waste DHD catalyst (7360) by reconditioning after previous peptization (Experiments in 100 cc furnace). Frames 350-353
14. Inhibition of dehydrogenation and permanent damage to DHD catalyst by oxygen-, nitrogen-, sulfur-compounds and unsaturateds. Frames 354-382
15. Test of DHD catalyst in 1 liter oven. Frames 383-395
16. Note on problem of second heating of DHD catalysts after saturation with ammonium molybdate. Frame 396
IV. Hochdruckversuche Laboratories. Papers on dehydrogenation. Files of frl. Dr. Horing.
Folder No. S32/VII-D-11.
1. Removal of sulfur dioxide for regeneration of DHD unit chambers. Frames 397-403
2. DHD gasoline, quality and yield, Ka. 807 Lu. Frames 404-409
3. Dehydration at 50 and 15 atm. Comparison of costs. Frames 410-421
4. Aviation spirit from Estonian shale oil. Frames 422-426
5. Hydrogenation and catalyst cracking of petroleum-gasoil catalytically cracked. Frames 427-433
V. Hochdruckversuche Laboratories. Papers on dehydrogenation. Files of Frl. Dr. Horing.
Folder No. S22/I-D-1.
1. On Ni-W-Dehydrogenation of gasolines rich in naphthene. 434 – 441
2. Experiments on catalyst for dehydrogenation (Experiments with 6434 gasolines from mineral coal liquefaction and mineral coal tar-middle oil.). Frames 442-449
3. On some possibilities of supplying heat in dehydrogenation of gasoline over 6718. Frames 450-456
4. Catalytic dehydrogenation of 5058 Scholven heavy stripper gasoline fraction 90-180°C and 7019 aromatization gasoline fraction 160-190°C over K 7360. Frames 457-461
5. DHD experiments in the 100 ltr. oven. 1st report: Processing of the fraction 160-190° from the 7019 aromatizing of mineral coal liquefaction middle oil in chamber 501. Frames 462-471
6. Dehydrogenation of fractions from 5058/6434 bituminous coal gasoline. Part I. Fraction 70-100° and 100-130°. Frames 472-480
7. Dehydrogenation under hydrogen pressure over moving catalyst. Report 9: Dehydrogenation of bituminous coal heavy gasoline “Scholven.” Report 481-492
VI. Hochdruckversuche Laboratories. Papers on hydrogenation of various coals. Files of Dr. Peters.
Folder No. S33/I-D-5.
1. Test of sample of Mathilde mine for suitability for hydrogenation (experiments in rotating autoclave). Frames 493-495
2. Valuation and preliminary hydrogenation results of samples of Rumanian coal in the autoclave by Prof. Heintze. Frames 496-499
3. Catalyst tests, particularly on influence of admixture of Na2S in hydrogenation of upper Silesian mineral coal in rotating autoclave. Frames 500-501
4. Decreasing and rising temperature in hydrogenation of upper Silesian coal. (Experiments in rotating autoclave). Frames 502-503
5. Hydrogenation behaviors of oxidized mineral coal in the autoclave at 600 atm. Frames 504-508
6. Hydrogenation results on two samples of wood tar from Sweden in the rotating autoclave. Frames 509-511
7. Janina coal. Present test results in rotating autoclave. Frames 512-514
8. Experiments on hydrogenation in rotating autoclave with ammonium-boro-flouride as catalyst for mineral coal. (Experiments at 300 and 600 atm in rotating autoclave). Frames 515-518
9. Hydrogenation results of two coal samples from pit “Gute Hoffnung” (formerly Jania), in rotating autoclave. Frames 519-522
10. Testing low temperature carbonizing residues of shale for their suitability as Sumpf phase catalysts. (Experiments at 600 atm in rotating autoclave.). Frames 523-526
11. Substitutes for ammonium chloride in hydrogenation of Scholven coal. (Experiments at 350 atm in rotating autoclave.). Frames 527-529
12. Early hydrogenation experiments with arsenic compounds. Frames 530-532
13. Hydrogenation experiments with gas purification agents of Ruhrgas A. G. in rotating autoclave. Frames 533-534
14. Early hydrogenation experiments with chlorinated and oxidized bituminous coal in an autoclave. Frames 535-540
15. Hydrogenation results with Janina coal (Auschwitz) K 1262 of 4-12-43 in rotating autoclave. Frames 541-545
16. Hydrogenation results with Myslowitz coal K 1263 in rotating autoclave at 350 and 600 atm pressure. Frames 546-548
17. Possibility of substituting ammonium chloride in the hydrogenation of Ruhr coal. (Early experimental results.). Frames 549-551
18. Preliminary hydrogenation results with elementary sulfur and various products. (Experiments in rotating autoclave). Frame 552
19. Experiments on isomerizing n-heptane over 5058 in a rotating autoclave. Frames 553-554
20. Early hydrogenation experiments in the autoclave with elemental sulfur. Frames 555-557
21. Experiments on hydrogenation of Spanish coal in rotating autoclave at 350 and 600 atm pressure. Frames 558-563
22. Results of experiments with Rhine soft coal in autoclave. Frames 564-565
23. Admixture of mineral coal tar pitch to Rhine brown coal (Experiments on hydrogenation in rotating autoclave). Frames 566-568
24. Experiments in autoclave on decomposition and hydrogenation of Estonian and other shale and shale concentrates. Frames 569-573
25. Experiments on decomposition of Bulgarian oil shale (Bresnik) (S 21) of 10-20-41 in the autoclave. Frames 574-575
26. Substituting iron sulfate by Lux mass or by Bayer mass ¸ H2SO4 in hydrogenation of Upper Silesian coal K 1242. (Experiments in rotating autoclave.). Frames 576-577
27. Note on formation of “Caviar” with Rhine brown coal. Analysis of ashes of Rhine brown coal. Frames 578-579
28. Influence of disposable hydrogen and volatiles on crude tar yield, and dependence of hydrogenation suitability on crude tar yield, from the hydrogen disposable and from volatiles in Upper Silesian- and Dombrown coal. Frames 580-582
29. Experiments on hydrogenation of concentrate of Estonian oil shale in rotating autoclave at 300 atm. Frames 583-584
30. Hydrogenation results of coal samples from Upper Silesian Fuerstengrube and Valeskagrube in the rotation autoclave. Frames 585-587.
30A. Examination of 2 generator dust samples from low temperature carbonization coke “Hercules” for their suitability as catalyst carriers. (Experiments in rotating autoclave). Frames 588-590
31. Hydrogenation suitability and carbonization value of Ruhr coals. Frames 591-592
32. Experiments on decomposing shale of the Messel pit (S 20) in rotary autoclave. Frames 593-594
33. Experiments on hydrogenation of old coal in rotary autoclave at 600 atm. Frames 595-599
34. Vanadium as catalyst in Sumpf phase. (Older and more recent experiments in rotary autoclave.). Frames 600-601
35. On the problem of pasting oil for the pressure extraction of mineral coal. Frames 602-606
36. Catalyst experiments with pitch mash “Welheim” in rotary autoclave at 600 atm. Frames 607-610
37. Processing of Estonian shale oil. Frames 611-614
38. Experiments on extraction in rotary autoclave for producing primary bitumen. Frames 615-625
39. Hydrogenation experiments for determining the influence if sulfur in Upper Silesian coal K 1180 and K 1197 in the rotary autoclave at 600 atm. Frames 625-633
VII. Hochdruckversuche Laboratories. Papers on foreign hydrogenation works. Files of Dr. Peters. Folder No. S33/I-C-5.
1. Notes on the conference of 22-8-40 at Paris (Rue Dr. Lanceraux) on the installation of the refinery in Gonfreville. Frames 634-637
2. Production of fuel in Northern France. Frames 639-640
3. Hydrogenation plant Lievin. Frames 641-650
4. Hydrogenation plant Bethune. Frames 651-666
5. Fischer (Tropsch) synthesis plant Courrieres-Kuhlmann. December 3, 1940. Frames 667-671. 6 pages.
6. Analyses of gasolines from Bethune and Lievin. Frames 672-674
7. Benzination of B-middle oil from Gardanne lignite coal. Frames 675-686
8. Catalytic pressure hydrogenation of Gardanne coal in small scale experiments at Ludwigshafen/Rhine. Frames 687-695
9. Yield from Gardanne coal. Frames 696-702
10. Report on a conference on the Japanese coal hydrogenation plant on 4-27-1944 at the “Laenderbank,” Berlin. Frames 703-705
11. Notes on a conference with the Japanese on preparing isooctane from isobutyl alcohol 7-22-1943 at Berlin. Frames 705-706
12. Quality of gasoline for Japan plant. Frames 707-710
VIII. Hochdruckversuche Laboratories. The coals of Upper Silesia. Files of Dr. Peters. Folder No. S33/I-C-6
1. The coals of the Upper Silesian coal area. Frames 711-727