T.O.M. Microfilm Reel 165
(Original Designation LF-67)
Table of Contents
Note from the editors – only selected documents from this microfilm reel have been completely processed and presented below in cleaned and grouped format (identified by HTML links below). The remainder of the reel is not related to the Fischer-Tropsch process, and therefore complete processing cannot be justified at this time.
We are, however, making the entire reel contents available in raw image format, although in a small number of relatively large files (rather than a very large number of small individual images). Anyone interested in pursuing the non-FT related material on this reel may find the document in these larger raw files.
Images 0001-0200 File size ca. 40 Mb
Images 0201-0400 File size ca. 39 Mb
Images 0401-0600 File size ca. 34 Mb
Images 0601-0800 File size ca. 43 Mb
Images 0801-0964 File size ca. 40 Mb
I. Reports on prehydrogenation.
II. Reports on aromatization.
III. Papers on octane numbers of aviation gasolines, etc.
IV. Papers on chemical equilibria.
V. Butan-tanol plant data. (not Hochdruckversuche Laboratories)
VI. Miscellaneous papers on hydrogenation of various coals in 10 liter furnaces.
VII. Some analytical methods. Files of Hochdruckversuche laboratories Lu 558. Determination nitrogen in middle oils, phenols in middle oils, viscosity at high pressures, miscellany.
Source of Documents: I.G. Central Library, Griesheim
Folder Nos. S-28/III-A-4
S-28/III-A-5
S-28/III-A-10
S-28/III-B-6
S-28/III-B-9
S-28/III-A-6
S-28/III-B-4
Filmed by: JIOA
Date: 10 Jan. 1946
I. Hochdruckversuche laboratories. Reports on prehydrogenation. Folder No.: S-28/III-A-4.
1. The effect of W, Ni, Co and Fe as active components on alumina pre-hydrogenation catalyst. Frames 1-9
2. Influence of the degree of hydrogenation (AP of B middle oil) on the results of 8376/6434 working of S-middle oil Scholven. Frames 10-20
3. The effect of W, V, Ni, Co and Fe as active components on alumina pre-hydrogenation catalysts. Frames 21-29
4. Use of the clay-W-Ni pre-hydrogenation catalyst 8376-7846 W 250 for various products. Frames 30-54
5. Testing of new pre-hydrogenation catalysts. Frames 55-58
6. Report on pre-hydrogenation test with middle oils from bituminous coal liquefaction over catalyst 7846 W. 250 on a semi-technical scale. Frames 59-82
7. Tests aiming at the pre-hydrogenation of bituminous coal liquefaction oil over catalyst 7846 W. 250. Frames 85-97
8. Use of the clay-W-Ni-pre-hydrogenation catalyst 8376 – 7846 for various products. Frames 98-132
9. Testing of new pre-hydrogenation catalysts in 50 cc lead bath furnaces. Frames 135-143
10. Hydrogenation activity of alumina-tungsten-nickel catalyst prepared in different ways. Frames 144-149
11. The influence of temperature on the results of the pre-hydrogenation with catalyst 7846. Frames 150-157
12. The influence of through-put, oil partial pressure and contact time on the results of pre-hydrogenation with catalyst 7846. Frames 158-170
13. Catalyst 7846 for pre-hydrogenation with middle oil Scholven. Frames 171-190
14. Further tests with alumina-Mo-Ni catalysts. Frames 191-198
15. Development of the pre-hydrogenation catalysts. Frames 199-221
16. Bases in pre-hydrogenation middle oils. Frames 222-224
17. Pre-hydrogenation catalyst tests. Frames 225-241
II. Hochdruckversuche laboratories. Reports on aromatization. Folder No.: S-28/III-A-5.
18. 600 at aromatization of bituminous coal liquefaction middle oils as preliminary stage in the production of DHD high efficiency motor fuels. Frames 242-255
19. Influence of the products partial pressure in the aromatization of bituminous coal liquefaction middle oil Scholven over alumina-Terrana catalyst 8688. Frames 256-260
20. Description of parallel experiments on a small scale as preparatory work for the large scale experiment in chamber 805 as well as a new continuous experiment concerning 600 at “Benzinierung” of bituminous coal liquefaction middle oil with Terrana catalysts. Frames 261-275
21. Influence of the recycle conditions on the 250 at aromatization of bituminous coal liquefaction middle oil over alumina-Terrana catalyst 8688. Frames 276-284
22. Aromatization at 250 atm with alumina-Terrana catalyst of the type 8688. Frames 285-298
23. The influence of the through-put on the 250 at aromatization of bituminous coal liquefaction middle oils with alumina-Terrana catalyst. Frames 299-305
24. The influence of pressure on the aromatization of bituminous coal liquefaction middle oil with alumina-Terrana catalyst. Frames 306-313
25. The influence of temperature and through-put on the 600 atm aromatization of bituminous coal liquefaction middle oil with Terrana catalyst. Frames 314-326
26. Comparison of benzination with natural bleaching earth (6109) and synthetic aluminum silicate (6752) at 600 atm. Frames 327-331
27. Influence of sulfur-addition on the single-stage 600 atm benzination of bituminous coal liquefaction middle oil with Terrana catalyst. Frames 332-336
28. Testing of new aromatization catalysts in 25 cc lead bath furnaces at 250 atm. Frames 337-341
29. Aromatization catalyst tests at 250 atm in 100 com lead bath furnaces (1. Report). Frames 342-356
30. Section testing of catalyst 7019 for the bleaching earth process. Frames 357-358
31. Aromatization at 250 atm. Development of catalysts. Frames 359-380
32. Catalytic tests concerning 250 and 600 atm aromatization in 1 liter furnaces with alumina, bleaching earth and synthetic silicate catalysts. Frames 381-397
33. Preparation of catalysts. Frames 398-402
34. Aromatization of middle oil derived from bituminous coal liquefaction. Frames 403-414
35. Note on the two stage production of gasoline rich in aromatics from bituminous coal liquefaction. Frames 415-418
36. Amount of catalyst 7019 lose in the normal operation with bituminous coal liquefaction middle oil. Frames 419-425
37. Once more the problem 300 versus 600 atm. Frames 426-427
III. Hochdruckversuche laboratories. Papers on octane numbers of aviation gasolines, etc. Folder No.: S-28/III-A-10/
38. The dependence of the mixture octane number on the starting gasoline. Frames 423-426
39. Octane numbers of the paraffins. Frames 427-436
40. Octane numbers of aromatics. Frames 437-446
41. Octane numbers of naphthenes. Frames 447-460
42. Calculation of octane numbers of gasolines. Frames 461-468
43. Aromatization catalysts at 250 and 600 atm. Frames 469-485
44. Note on the aromatization at 250 and 600 atm. Frames 484-491
45. Utilization of UO2 in aromatization catalysts. Frames 492-499
46. Dehydrogenation tests at atmospheric pressure aiming at testing aromatization catalysts. Frames 500-502
47. Dehydration experiments for testing aromatization catalysts. Frames 503-505
48. Aromatization of various middle oils at 600 atm over catalyst 7495 (Welheim) in the 1,2 liter furnace. Frames 506-517
49. Influence of (various) catalyst components on aromatization. Frames 518-522
IV. Hochdruckversuche laboratories. Papers on chemical equilibria. Folder No. S-28/III-B-6.
50. Aromatics – Naphthenes equilibrium. Frames 523-534
51. Note on the conversion of sodium carbonate into sodium sulfide during the sulfurization of the Bayer mass by means of either pure hydrogen sulfide or a mixture of hydrogen sulfide and carbon dioxide. Frames 535-536
52. The position of the equilibrium during the dehydrogenation of cycloparaffins to aromatics. Frames 537-542
53. Thermodynamic data on bondage and stability of hydrocarbons. Frames 543-560
54. Some pressure hydrogenation equilibria calculated by means of Nernst’ approximation formula. Frames 561-564
56. The possibility of formation and reduction of iron and chromium nitrides under hydrogenation conditions. Frames 573-577
V. Butan-tanol plant data. Folder No. S-28/III-B-9.
57. Installation of a butanol-tanol experimental plant of approximately 20,000 tons per year capacity E T 100 at Heydebreck. Frames 578-584
58. Butane dehydrogenation (74,000 tons per year). Rough estimate of requirements. Frame 585
59. Butane dehydrogenation. Frames 586-590
VI. Miscellaneous papers on hydrogenation of various coals in 10 liter furnaces. Folder No.: S-28/III-A-6.
60. Working of Scholven coal (Zweckel-coal) with iron catalysts and chlorine. Frames 591-593
61. The working of coal plus low carbonization tar for fuel oil and briquetting agents. Frames 594-595
62. Development of the test carried out with topped Brux tar in the 10 Liter furnace. Frame 596
63. Working of Silesian coal “K 1180” Beutehn mine for gasoline and middle oil at 600 atm in the 10 liter furnace (411 and 451). Frames 597-645
64. Working of Silesian bituminous coal 1160 (Preussen mine) to an excess of heavy oil at 600 atm. in the 10 liter furnace. Frames 644-674
65. Middle oil concentration in the bituminous coal sumpf phase under different conditions of operation. Frame 675
66. Heating of coal paste (experimental work). Frames 676-693
67. Sampling and methods of analysis (10 liter furnace). Frames 694-703
68. Working of Silesian coal “K 1174” to an excess in heavy oil at 600 at. in the 10 liter Furnace. Frames 704-735
69. Hydrogenation of old coals. Frame 736
70. Working of Silesian coal “K 1160” (Prussian mine) to gasoline and middle oil at 600 atm in the 10 liter. furnace. Frames 737-763
71. The influence of the middle oil content in the diluent oil on the composition of the newly formed product in the working of Silesian coal K 1197 under different conditions of operation. Frames 764-768
72. Working of Silesian coal form the Heinitz mine for a high excess in heavy oil with a simultaneous, extensive decomposition of the asphalt content. Frames 769-771
73. Sumpf phase gasolines obtained from Silesian bituminous coal under different conditions of operation. Frames 772-773
74. Status of the experiments in the 10 Liter furnaces. Frame 774
75. Working up of residue on the industrial scale and in the 10 liter furnace. Frames 775-776
76. Composition of the gases in working Silesian bituminous coal and bituminous coal high temperature tars at 600 atm for heavy oil. Frames 777-778
77. The use of very large through-put in the working of Silesian coal for a maximum excess in heavy oil. Frames 779-782
78. Working of Silesian coal “K 1174” for gasoline and middle oil at 600 at. in the 10 liter furnace. Frames 783-817
79 Working of bituminous coal for varying amounts of heavy oil excess. Frames 818-823
80. Silesian bituminous coal 1118 worked for gasoline and middle oil at 600 at in the 10 liter furnace. Frames 824-856
81. Hydrogenation of not previously de-ashed Upper Silesian coal in the presence of chlorine. Frames 857-861
82. Hydrogenation under pressure of Upper Silesian coal from the Heinitz mine in the 10 liter Furnace with stirrer. Frames 862-865
83. Experimental methods applicable to the 10 liter furnaces in the Sumpf phase. Frames 866-872
84. Apparatus constants of the 10 liter furnaces. Frames 873-876
85. Comparison of the 10 liter coal furnace with large scale technique. Frames 877-878
86. Sumpf phase hydrogenation of the Sudeton coal “Herkules” in the 1- liter furnace at 250 and 600 atm. Frames 879-916
87. Pressure hydrogenation of young coal from Gelsenberg at 600 atm. to gasoline and heating oil, respectively to heavy Diesel oil, in the 1- liter furnace. Frames 917-922
VII. Some analytical methods. Files of Hochdruckversuche laboratories Lu 558. Determination nitrogen in middle oils, phenols in middle oils, viscosity at high pressures, miscellany. Folder No. S-28/III-B-4.
88. Conference in Gelsenberg. 16 and 17 Feb. 1944. Nitrogen determination in middle oil. Frames 923-925
89. Directions for the determination of basic nitrogen in middle oils by means of titration with perchloric acid in concentrated acetic acid. Frames 926-932
90. An exact, potentriometric and quick determination of basis nitrogen in middle oils. Frames 935-945
91. Determination of the nitrogen contents of middle oils. Frames 946-954
92. Phenol determination in middle oils. Frames 955-956
93. High pressure viscosity meter. Frames 957-962
94. Literature on coke tests (Conradson and Ramsbottom tests). Frames 965-966
95. Asphalt determination in sludge. Frame 967