T.O M. Microfilm Reel 164
(Original Designation LF-63)
Table of Contents
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Miscellaneous Reports On Hydrogenation, Hochdruckverfahren Laboratories, I. G. Farben A. G.
Source of Documents: Griesheim Central I. G. Library
Folder Nos.:
S-15/III-A-6,5,7,9
S-15/II-E-8,1,5,3
S-15/II-D-3,4,9,11,10
S-15/II-B-11
Filmed by: JIOA
Date: Jan. 7, 1946
I. Hochdruckverfahren Laboratories: Miscellaneous Office - Reports and Papers. Folder No.: S-15/III-A-6.
1. Working of middle oils over dehydrogenation catalysts III. Working of pre-hydrogenation and aromatization middle oils over catalyst 8147. Frames 1-7
2. Aromatization contact for 600 at from previously used 6434. Frames 8-16
3. Report on the conference establishing the arrangement of apparatus for the large scale experiments in chamber 804. Frames 17-20
4. “Benzinierungs” catalysts with HF-treated alumina (clay) as carrier. Frames 21-25
5. Exchange of experience in analytical methods at Ludwigshafen, 10 June 1941.Frames 26-34
6. Determination of the contents in aromatics of Gasolines according to the aniline point method. Frames 35-52
7. Direction for the determination of the aromatics-content in gasolines by the aniline point method. Frames 43-47
II. Hochdruckverfahren Laboratories: Miscellaneous Office Reports and Papers. Folder No.: S-15/III-A-5.
1. Production of DHD-benzine from 5058/6434 gasoline Scholven at Ludwigshafen, chamber 504. Frames 48 – 87
2. Dehydrogenation of aromatization heavy gasoline. Tests in the 1 ltr. furnace with K 7994 (light alumina (clay) plus 2% Mg0 plus 12% Mo0). Frames 88-99
3. The influence of the middle oil contents in the diluent oil on the composition of the newly formed products during the treatment of Silesian coal K 1197 under various conditions. Frames 100-107
4. Flowsheet of an alkylation plant. Frames 108-110
5. Overload curves and chemical constitution of the fuels. Frames 111-118
6. Nitride formation on chromium steels during the high pressure gasoline synthesis and its prevention. Frames 119-122
7. Experiments of the Anic (?) with fluoride catalysts. Frames 123-129
8. New pre-hydrogenation catalysts prepared by diluting 5058 with ZnS. Frames 130-132
9. Calculation of the heat of reaction in dehydrogenation reactions. Frames 133-142
III. Hochdruckverfahren Laboratories: Miscellaneous Office Reports and Papers. Folder No.: S-15/III-A-7.
3. Tests on the heating up of coal paste. Frames 167-185
4. Aromatization tests at 45 atm. with a catalyst of decreasing activity. Frames 186-189
5. Determination of solid aromatics in a residue from pitch hydrogenation Politz. Frames 190-192
IV. Hochdruckverfahren Laboratories: Miscellaneous Office Reports and Papers. Folder No.: S-15/III-A-9.
2. Analysis, separation and hydrogenation of the components of coal structure (Quotations from the literature). Frames 214-226
3. Aromatization of bituminous coal liquefaction middle oil with additions of sumpf gasoline at 600 atm. over bleaching earth catalysts. Frames 227-234
5. Hydrogenation tests with coals of different petrographic composition in rotary autoclaves. Frames 238-242
6. Report of the committee dealing with problems of quality and planning. Frames 243-256
V. Hochdruckverfahren Laboratories: Miscellaneous Office Reports and Papers. Folder No.: S-15/II-E-8.
1. Dependability of the capability of oils to be “benziniert” on their nitrogen content. Frames 257-265
2. Comparison of the dewaxing plant at Lutzkendorf with the experimental plant at Ludwigshafen. Frames 266-270
3. Production of 20,000 tons/mth aviation gasoline at Gelsenberg by means of catalytic cracking. Frames 271-274
4. Some pressure hydrogenation equilibria, calculated by means of the approximation formula of Nernst. Frames 275-277
VI. Hochdruckverfahren Laboratories: Miscellaneous Office Reports and Papers. Folder No.: S-15/II-E-8.
1. The formation of unsaturated hydrocarbons in the carbon monoxide hydrogenation (Fischer-Tropsch synthesis). By Henkels. December 15, 1941. Frames 278-283. 7 pages.
2. Present status of the DHD-plants Ludwigshafen/Opplitz and Politz. Frames 284-295
3. Small scale experiments in propane dewaxing. Frames 296-318
4. Exchange of (Fischer-Tropsch synthesis) experience (conference) on December 4, 1941 at Ludwigshafen/Rhein. Frames 319-349. 32 pages.
5. Low pressure splitting of (50 atm) petroleum middle oils. Frames 350-369
6. Tests for the improvement of lube oils by means of catalysts 8376. Comparison with catalyst 5058. Frames 370-382
7. Chemical high pressure processes. Frames 383-392
VII. Hochdruckverfahren Laboratories: Miscellaneous Office Reports and Papers. Folder No.: S-15/III-A-9.
1. Processes for the production of knock-resistant hydrocarbons. Frames 393-408
2. Working method of the deparaffination plant at Lutzkendorf. Frames 409-411
3. Further sludge filtration tests with various solvents. Frames 412-415
4. Specific heats. Frames 416-427
5. “Benzinierung” of catalyst 6434: Dependence of gasification, efficiency, octane numbers, etc. on the gasoline end point and the through-put, using petroleum middle oil feed. Frames 428-443
6. Temperature measurement in the Sumpf phase furnaces. Frames 444-446
7. Production of DHD-gasoline from 5058 prehydrogenation gasoline of the hydrogenation plant Merseburg. Frames 447-480
8. Filtration of hydrogenation sludge with addition of sulfite lye. Frames 481-483
9. Institutes and research-workers in the U.S.S.R. who are engaged in the working up and particularly in the hydrogenation of coals, tars and petroleum oils. Frames 484-485
10. Production figures of various hydrogenation plants during October 1941. Frames 486-488
11. Propane filter. Frames 489-490
12. Cyclohexane. Frames 491-493
VIII. Hochdruckverfahren Laboratories: Miscellaneous Office Reports and Papers. Folder No.: S-15/II-D-3/
1. Gas phase, large scale experiment 1939. Chamber Treatment of bituminous coal liquefaction middle oil and bituminous coal tar middle oil for aromatic gasoline CV 2b and CV 5b over catalyst 7019 L 8. Frames 494-499
2. Aromatic hydrocarbons in hydrogenation products. Frames 500-503
3. Polycyclic solid aromatics from hydrogenation products. Frames 504-512
4. Concerns: Oxo process. Frames 513-523
5. Comparison of the 10 ltr. coal furnace with large scale technique. Frames 524-525
IX. Hochdruckverfahren Laboratories: Miscellaneous Office Reports and Papers. Folder No.: S-15/II-D-4.
1. Stability of carbazol during hydrogenation. Frames 526-527
2. Polycyclic, aromatic compounds in various tars and crude oils. Frames 528-535
3. Hydrogenation of anthracene residues. Frames 536-538
4. Theory of decomposition (dis-integration) of coal derivatives (humic acid derivatives) in Sumpf and gaseous phase. Frames 539-544
5. Solubility of corenes and benzoperylene at 20°C. Frame 545
6. Oxidation experiments and use of oxidation products according to the stage reached on 1 April 1940. Frames 546-550
X. Hochdruckverfahren Laboratories: Miscellaneous Office Reports and Papers. Folder No.: S-15/II-D-9.
1. Directions for the orientating analysis of oil shale. Frames 551-560
2. Observation on catalysts, particularly cracking catalysts. Frames 561-565
3. Ageing symptoms of insulating oils. Frames 566-574
XI. Hochdruckverfahren Laboratories: Miscellaneous Office Reports and Papers. Folder No.: S-15/II-E-5.
1. Exchange of experience. Welding in the interior of used benzination and coal furnaces. Frames 575-580
XII. Hochdruckverfahren Laboratories: Miscellaneous Office Reports and Papers. Folder No.: S-15/II-D-11.
1. Furnace 504. Change to regeneration. Frames 585-589. 6 pages, virtually illegible.
3. High efficiency motor fuels. Frames 600-628
4. Method for the approximated calculation of overload curves from the octane number of the rest gasoline and from the contents in aromatics. Frames 629-637
5. Another statement on the question 300 versus 600 atm. Frames 658-659
6. Tests on sludge filtration. 640-648
XIII. Hochdruckverfahren Laboratories: Miscellaneous Office Reports and Papers. Folder No.: S-15/II-E-1.
1. Hydrogenation, splitting hydrogenation and cracking of kybol and kybol residues. Frames 649-657
2. Direct “Benzinierung” of bituminous coal liquefaction middle oil over catalysts 6454 at 600 atm. Frames 658-661A
3. Study of the use of 700 or 300 atm in the gaseous phase. Frames 662-666
4. Composition of off-gases in “Benzinierung” and aromatization. Frames 667-679
5. A statement on the question 300 versus 700 atm. for Upper Silesia. Frames 680-688
6. Cracking experiments over K 6108 (Terrana HF) under different pressure conditions. Frames 689-716
7. Cracking of gasoline and gas under hydrogen pressure. Frames 716A-716Q
XIV. Hochdruckverfahren Laboratories: Miscellaneous Office Reports and Papers. Folder No.: S-15/11-D-10.
1. Theoretical meaning of overload curves. Frames 717-728
2. Development of dehydrogenation catalysts. Part III. Alumina, - Me-Ni-catalysts. Frames 729-751
XV. Hochdruckverfahren Laboratories: Miscellaneous Office Reports and Papers. Folder No. S-15/III-B-11/
1. The influence of catalyst pressure and product partial pressure during cracking and hydrogenation of Bruchsal gas oil. Frames 752-760
2. Laboratory and works experiments aiming at increasing the yield in low carbonization oil during the low temperature carbonization of asphalt bearing residue. 12 May 1943. Dr. Horn/Dr. Hinz. Frames 761-763
3. Installation of a new oil tank. Frame 764
4. Influence of the products partial pressure in the aromatization of bituminous coal liquefaction middle oil Scholven over alumina (clay) – Terrana contact 8688. Frames 765-768A
5. Hydrogenation results in the rotary autoclave with (coal) samples from the Radzionkau mine in Upper Silesia. Frames 769-772
6. Hydrogenation experiments with Spanish coals in the rotary autoclave. Frames 773-775
7. Working of primary bitumen to heavy oil. Frames 776-779
8. Present attitude on the report of the hydrogenation works Politz about experiments aiming at increasing the low temperature carbonization yield by means of sulfur addition. Frames 780-783
9. Isolation and determination of coronen in hydrogenation residues. Frame 784
10. Sodium sulfide production. Frames 785-786
11. The chemical composition of the crusts forming on the preheaters. Frames 787-789
12. Brief report by Schapper on occasion of the exchange of experience on 22 March 1943. Frames 790-793
13. Reducing the stress on the Sumpf phase preheaters. Frames 794-806
14. Isolation and determination of coronen in pitch and hydrogenation residues. Frames 807-808
15. Pyridine in Sumpf phase gasoline. Frame 809
16. Hydrogenation experiments in the rotary autoclave with Brux tar (P 1397 original). Frames 810-815
17. Improvements in an experimental apparatus for working with powder catalyst. Frames 816-820
18. Worker recruitment for the army. Frames 821-822
19. Quarterly reports on hydrogenation catalysts. Frames 823-827
20. Chemical problems connected with the heating up of bituminous coal paste. Frame 828
21. Activity report February – March 1943. Frames 829-843
22. Experiments in a 100 com furnace aiming at the preparation of pure aromatics, particularly toluol from xylol and DHD residue. Frames 844-848
23. Conversations regarding de-ashing of coal. Frame 849
24. Propane de-waxing. Frames 850-852
25. Hydrogenation plant in Teruel (Spain). Frames 853-854
26. Hydrogenation tests with Puertollano coal K 1253 in the rotary autoclave. Frames 855-859
27. Regeneration of coal paste diluted with middle oil. Frames 860-861
28. Steam cylinder oil with low pour point. Frames 862-864
29. Discussion at the Reichsforschungerat. Frames 865-866
30. Quarterly reports on Hydrogenation catalysts Scholven. Frames 867-869
31. Comparison of the carbon and iron consumption for bituminous coal hydrogenation and for carbonization followed by hydrogenation. Frames 870-872
XVI. Hochdruckverfahren Laboratories: Miscellaneous Office Reports and Papers. Folder No. S-15/II-E-3.
1. Reduction equilibrias (hydrogen fluoride partial pressures) of fluorides with regard to their catalytic action. Frames 873-885
2. Experiments with models concerning the dilution of lubricants. Frames 886-900
3. Reaction of carbon monoxide with hydrocarbons. Frames 901-905