T.O.M. Microfilm Reel 162
(Original Designation LF-46)
Table of Contents
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Source of documents: Griesheim Central I. G. Library
Folder Nos.
S-1/I-D-6
S-35/I-C-10
S-15/III-B-9
S-15/III-B-8
S-15/III-C-1
S-15/III-B-12
S-15/III-B-12
S-15/III-B-7
S-15/III-B-6
Filmed by: JIOA
Date: December 28, 1945
Section I. I. G. Farbenindustrie Reports About Pressure Distillation, Electrode Coke, Catalytic Cracking,
File Of Prof. Dr. Horing
Source of
Documents: Griesheim I. G. Central
Folder Nos:
S-1/I-D-6
Filmed by:
JIOA
Date:
December 28, 1945
1. Molecular compounds of coronen with Coronen derivatives. Frame 1
2. Pressure distillation of various raw materials. Frames 2-3
3. Pressure distillation apparatus and required amounts. Frame 4
4. Process of pressure distillation. Frames 5-12
5. Pressure distillation of Pechelbronner 01. Frames 13-16
6. Pressure distillation of Pechelbronner 01. Frames 17-21
7. Chemical effect and the influence of catalysts in pressure distillation. Frames 22-28
8. Balance for L-Gasoline from brown coal tar via 300 atmosphere hydrogenation and catalytic cracking for gasoline. Frames 29-30
9. Catalytic cracking (appraisal of solid and fluid catalysts). Frames 31-34
10. Cracking experiments with Si-Al-catalysts (K-6752) in a 50 liter furnace and comparison of the results with the K 6108 fluid catalyst process. Frames 35-71
11. Fuel oil from low temperature carbonization tar via pressure distillation. Frames 72-74
12. Comparison of the most important thermal Cracking process with pressure distillation. Frames 75-79
13. The influence of flow velocity and the effect of gas additions in pressure distillation. Frames 80-86
14. Catalytic cracking of various middle oils for L-gasolines. Frames 87-99
15. Expansion of the M.B.B. catalytic cracking and gasphase hydrogenation installation. Frames 100-103
16. A new combination process for the increase of L-gasoline yield in catalytic cracking. Frames 104-106
17. Production of 20,000 tons/month L-gasoline at Gelsenberg via catalytic cracking. Frames 107-110
18. Catalytic cracking of middle oils in the presence of aluminum chloride. Frames 111-125
19. Preliminary plans for a catalytic cracking installation. Frames 126-131
20. New composition and price of production for new leather fatting material. Frame 132
21. Addenda to the cost estimate for the oxidation of oil according to Pfirrmann. Frames 133-135
22. Electrode coke. Frames 136-137
23. Production of electrode coke in Upper Silesia. Frames 138-141
24. Electrode coke for rectifiers. Frame 142
25. Discussion about binders on Feb. 2, 1943. Frames 143-147
26. Improvement of the binding properties of bitumen by oxidation. Frame 148
27. Hydrogenation residues as starting material for electrode coke and briquette binding. Frames 149-152
28. Discussion on electrode coke held in the Landerbank at Berlin on Dec. 3, 1942. Frames 153-156
29. Status of electrode coke production via extractive hydrogenation. Frames 157-160
30. Electrode coke. Frames 161-163
31. First estimates on the working up of primary bitumen by hydrogenation. Frames 164-166
32. On the possibility of commercial electrode coke by means of extractive hydrogenation. Frames 167-169
33. Production of electrode coke from hydrogenation products and of other raw materials. Frames 170-172
34. Extractive hydrogenation in a 10 C furnace. Frames 173-177
35. Electrode coke via primary bitumen. Frame 178
36. Regarding the filtration of hydrogenation residues from Chamber 804 at 700 atmospheres and 25 MV by dilution with middle oil. Frames 179-181
37. Regarding the filtration of hydrogenation residues from Chamber 804 at 700 atmospheres and 25 MV by dilution with middles oil. Frames 182-186
38. Anode materials for rectifiers. Frames 187-188
39. Anode materials for rectifiers. Frames 189-190
40. Cost estimate :z-Bi + Ni + Electrode coke. Frames 191-196
41. Production of electrode coke by thermal cracking under pressure. Frames 197-199
42. Present results of the large-scale experiment Chamber 804 for the product of low ash primary bitumen for electrode coke production. Frames 200-205
43. Filtration of Chamber 804 residue in the process for preparation of primary bitumen. Frames 206-210
44. Report on a visit to the aluminum plant at Bitterfeld. Frames 211-214
45. Topped hydrogenation residue Scholven as briquetting material as a substitute for pitch in the production of electrode coke. Frames 215 – 216
46. In ref: electrode coke production at Blechhammer. Frames 217-219
47. Primary bitumen for the bitumen, sack and rubber industries. Frames 220-221
48. Equipment for carrying out filtration experiments. Frames 222-223
49. Working Silesian coal for heavy oil and electrode coke. Frame 224
50. Remarks on filtration experiments from the year 1937. Frames 225-227
51. The production of electrode coke and low temperature coal tar of low pour point by low temperature carbonization of primary bitumen. Frames 228-230
52. Experiments for the production of primary bitumen for the manufacture of electrode code. Frames 231-234
53. Influencing factors on filtration velocity of bituminous hydrogenation products. Frames 235-238
54. Filtration of slightly hydrogenated coal. Frames 239-241
55. Cost comparison of lubricating oil and primary bitumen then filtered on commercial pressure filters. Frames 242-247
56. Influence on the price of coal on the cost of manufacture of primary bitumen. Frames 248-251
57. In re: electrode coke. Frames 252-254
58. De-ashing of brown coal and bituminous coal for the production of electrode coke. Frames 255-256
59. Electrode coke. Frames 257-258
60. Production of electrode coke via pressure distillation. Frame 259
61. Experiments on the production of electrode coke. Frames 260-263
62. The production of ash-free electrode coke via primary bitumen. Frames 264-270.
Section II. Files Of I. G. Hochdruck Laboratories On Various Phases Of Catalytic Cracking.
Source of
documents: Griesheim I. G. Central Library
Folder No.:
S-33/I-C-10
Filmed by:
JIOA
Date:
December 28, 1945
1. Examination of magnesium silicate contacts by the Standard Oil Company. Frames 271-278
2. Esso Laboratories. Catalyst cracking with Powdered catalysts. Frames 279-282
3. Catalytic cracking. Preparation of synthetic cracking catalysts. Frames 283-284
4. Standard Oil Development Company Process Department. Report on cracking with large concentration of suspended powdered catalysts. Report Nr. 1. Frames 285-286
5. Extract from report No. 16 (15.3.1939) of the Esso Laboratories. The development of contacts for catalytic cracking. Frame 287
6. Standard Oil of Indiana: Summaries of reports on “Catalytic Refining”. Frames 288-289
7. The M. W. Kellog Company, New York 14725/10 22.9.38. The effect of parallel and countercurrent as well as that of pressure on catalytic cracking. Frames 290-293
8. Conference in Ludwigshafen 558 on the catalytic treatment of oil on 23 and 24 May 1939. Frames 294-308
9. Report on the conference in Leuna on the 24 and 25 January 1939. Catalytic dehydrogenation of naphthenes and catalytic dehydrogenation of normal and iso C4H10. Frames 309-324
Section III. Office Reports On Various Phases Of Hydrogenation. Hochdruckverfahren Laboratories.
Source of
Documents: Griesheim I. G. Central Library
Folder No:
F-15/III-B-9
Filmed by:
JIOA
Date:
December 28, 1945
2. The influence of the sulfur addition during the aromatization of middle oil from coal liquefaction over alumina (clay) – terrana contact at 250 atm. Frame 327.
3. DHD-contact examinations in 100 ccm-ovens. Frames 328-336
4. Hydrogenation by Dr. M. Pier. Frames 337-359
5. Some comparative hydrogenation plant data. (Report on a meeting). Frames 360-363
6. Fluorescence and phosphorescence. Frame 364
7. Hair pins for gas heated preheaters. Frame 365
9. Coronen. Frame 370
10. Survey over the measuring and regulating instruments used in hydrogenation, dehydrogenation and methanol synthesis. Frames 371-372
11. Heat of reaction and hydrogen requirements. Frames 373-376
12. About the regeneration of coal-lye with middle oil dilution. Frames 377-381
13. De-paraffination tests on a rotating filter with TTH-residue from Zeitz. Semi-technical scale. Frame 382
14. Conference on 15 February 1943. Requirements and consumption of various materials at the hydrogenation works at Magdeburg. Frames 383-389
15. Concerns: Project Spain. Plans for the installation of the De-paraffination plant. Frames 390-391
16. Flue-gases of the DHD-toluol plant Ludwigshafen/Opladen after the second reconstruction (enlargement). Frames 392-400
17. Influence of added organic nitrogen compounds on the results of the “benzinierung” of petroleum-gas oil over contact 6434. Frames 401-405
18. Problems relating to materials of construction in the hydrogenation process. Frames 406-407
19. Examination of DHD-contacts in the 1 liter oven. Frames 408-422
20. Pyridine production from brown coal sediment phase-products. Preliminary tests. Frames 423-426
21. Conference in Ludwigshafen on the 5 February 1943 on the production of phenol from distillation tar. Frames 427-430
22. Briquetting material from hydrogenation residues of the hydrogenation plant “Rheinbraun”. Frames 431-437
23. Briquetting tests with brown coal Hypech (Br. Hypech) from the Union Rheinische Braunkohlen Kraftstoff A.G. Wesseling (Bonn) in the briquetting laboratory 14 to 22, 9 1942. Investigator: Dipl. Ing. Mueller. Frames 438-447
24. Report B 29 about the briquetting tests with brown coal-Hypech (end) from the Union Rheinische Kraftstoff A. G. Wesseling, Bonn, in the briquetting laboratory, 18. to 23.11.1942. Frames 448-455
25. Working up of Boehlener tar at 250 at. In a 10 ltr. Oven. Frames 456-471
27 Report on activities from December 1942-January 1943. Frames 477-486.
A. Examination of catalyst for the terra alba process, Ludwigshafen.
B. Examination of catalyst for the terra alba process, Poelitz.
C. New catalysts for production of synthetic benzene.
D. New contact for aromatization at 250 at.
E. Controlled aromatization at 600 at.
F. Preliminary hydrogenation.
G. Benzination of P 1251/7846/8754-C- middle oil.
H. Benzination of P 1522 (crude paraffin Lutzkendorf) 6434 (600 at) B-middle oil
I. Working up of Spanish (Puertollano) shale middle oil.
K. Experiments aiming at the improvement of paraffins.
L. Splitting of bituminous stripper heavy oil vacuum distillate over fixed bed catalysts at 600 at.
M. Demethylation of xylol.
N. Experiments in the rotary autoclave.
29. Experiments carried out both in the laboratory and in the works aiming at increasing the yield in coal tar during the low temperature carbonization of bituminous residues. 12.5.1942. Dr. Horn/Dr. Hinz. Frames 490-501
30. Benzination of DHD-residue. Frames 502-526
31. Sieving analysis of coal and coal paste. Frames 527-528
32. The starting of new gas-phase catalysts. Frames 529-530
33. Deparaffination Zeitz. Frames 531-532
34. The benzol-insoluble in briquetting and binding agents. Frames 533-536
Section IV. Miscellaneous Topics Relating To Various Phases Of Hydrogenation.
Source of
Documents: Griesheim I.G. Central
Folder No:
S15/III-B-8
Filmed by:
JIOA
Date:
December 28, 1945
1. Binding agents and their composition. Frames 537-543
2. Pressure hydrogenation of dry coal. Frames 544-549
3. DHD-tests in a 40- ltr.-furnace. (3 DHD-furnaces with intermediate heating, 1 raffination furnace). Working of 6434- Benzene Scholven into high performance benzene. Frames 550-566
4. Hydrogenation tests in the autoclave with acid resin bitumen from Pape & Co. and with a soft asphalt from Dollbergen. Frames 567-571
5. Approximated calculation of the heat transfer number of a preheater. Frames 572-576
6. Electric pre-heater. Frames 577-580
7. Orientating hydrogenation tests with Hansa extract (P 1552 from the 18.11.42) from cellulose Waldhof. Frames 581-583
9. Investigations on the binding agent in the manufacture of coal. Frames 587-607
10. Present state of the tests with Benzene inhibitors. Frame 608
11. A new preparation of toluol from benzene. Frames 609-611
12. DHD-catalyst examinations in a low Com furnace. 9. report. Frames 612-625
13. Notes on the preparation of 5058 for TTH-Zeitz. Frames 626-627
14. The influence of the nitrogen content of oils on their capability to be “benziniert.” Frames 628-635
Section V. Various Office Reports On Fuel Synthesis Processes At Hochdruckverfahren Laboratories
Source of
Documents: Griesheim I. G. Central Library
Folder No:
S15/III-C-1
Filmed by:
JIOA
Date:
December 28, 1945
1. The working of bituminous high temperature coal tar with additions of bituminous coal. Frames 636- 658
2. Hydrogenation, dehydrogenation and splitting of coronen with WS2 (B. Bomb-tests). Frames 659-664
3. The occurrence of intermediate amorphous stages during the production of WS2 catalyst via ammonium sulfotungstate. Frames 665-666
4. Directions for the mode of construction of hydrogenation chambers. Frame 667
5. WS2 during the splitting without pressure. Frames 668-677
6. The use of molybdenum-and tungsten sulfide as catalysts for pressure hydrogenation. Frames 678-686
8. Aromatics-naphthenes equilibrium. Frames 692-695
9. Basic data for the comparison of a Bituminous coal hydrogenation with a low temperature bituminous coal carbonization. Frame 696
10. Production of catalyst 6434. Frames 697-698
11. Tests aiming at the establishment of the aromatics-naphthene equilibrium over the tungsten sulfide catalyst 5058. Frames 699-700.
12. Working of bituminous coal middle oil by means of preliminary hydrogenation/7846 W. 250. “Benzinierung” and DHD. Frames 701-718
13. Production of toluol from xylol and from “the residue from the Witol distillation Waldenburg.” Frames 719-735
14. Differences between various raffination methods for bituminous coal. Frames 736-738
15. Concentration-determinations of soft and hard pastes with the Brabender plastograph. Frames 739-751
16. The effect of sulfur during the catalytic high pressure hydrogenation. Frames 752-753
Section VI. Miscellaneous Office Records Of Hochdruckverfahren Laboratories
Source of
Documents: Griesheim I. G. Central Library
Folder No:
S15/III-B-12
Filmed by:
JIOA
Date:
December 28, 1945
1. Notes on the critic offered by F.A.F. Schmidt on the research work of the Strasburg Institute. Frames 754-755
3. Theory of the ammonia catalysts. Frames 766-773
4. Iron sulfate as catalyst for bituminous coal. Frames 774-780
5. Synthetic standard materials for overloading examination. The dependence of overload curves on the contents in naphthene. Frames 781-786
6. Tests related to the production of toluol by dehydrogenation of fractions of a DHD-stripper from bituminous coal and subsequent final distillation of the dehydrogenated products. Frames 787-802
7. Working up TTH obtained from low temperature carbonization Lugir-tar from Puertollano-oil shale. Frames 803-815
8. Methylcyclopentane from benzene or cyclohexane. Frames 816-819
9. Meeting report on the problem of replacing cobalt by iron. April 19, 1943. Frames 820-821. 2 pages.
10. Meeting report on the problem of replacing cobalt by iron. April 19, 1943. Frames 822-825. 5 pages.
11. Influence of the contents in nitrogen on the capability to be “benziniert” and on the nitrogen determination. Frames 826-837
12. Highly condensed aromatics; asphalts and contacts. Frames 838-840
13. Hydrogenation experiments with Spanish coals in the rotary autoclave. (Intermediate results). Frames 841-843
14. WS2 as catalyst for the prehydrogenation of polynuclear aromatics. Frame 844
13. Tungsten sulfide catalyst. Frame 845-846
14. Hydrogenative treatment of specially hard waxes of Fischer’s synthesis over catalysts 8376 at 250 at. Frames 847-869
15. Increasing the low temperature carbonized yield by additions of catalyst and excess of steam. Frames 870-876
16. Production of 5058 on a technical scale. Frames 877-878
17. Production of slightly hydrogenated coal. Frames 879-885
18. Construction mode of hydrogenation chambers. Frames 886-893
19. Determination of phenol in middle oils.
20. Crystal structure and X-ray examinations of the WS2-catalyst.
21. Appendix to the report on “Laboratory experiments aiming at increasing the yield in low carbonization product during the low temperature carbonization of bituminous (asphalt-containing) residues.” Frames 898-900
Section VII. Miscellaneous Office File Of Hochdruckverfahren Laboratories
Source of
Documents: Griesheim I. G. Central Library
Folder No:
S15/III-B-7
Filmed by:
JIOA
Date:
December 28, 1945
1. The washing out of sulfur dioxide during the regeneration of the DHD-unit chambers. Frames 901-907
2. The influence of pressure during the aromatization of bituminous coal liquefaction middle oils with Terrana-catalyst. Frames 908-915
3. Quick determination of lead in aviation fuels according to DVL (simplified method). Frames 916-920
Section VIII. Miscellaneous Office File Of Hochdruckverfahren Laboratories
Source of
Documents: Griesheim I. G. Central Library
Folder No:
S15/III-B-76
Filmed by:
JIOA
Date:
December 28, 1945
1. Present state of the tests aiming at the production of fatting agents for the top leather in military equipment. Frames 921-924
2. Knocking tests with aromatic mixtures. (Continuation of the survey from the 9.10.42). Frames 925-934
3. DHD-catalyst examinations in 100 com furnaces. 8. report. Frames 935-942
4. Maximum liquid gas production from stabilization waste gases. Frames 943-959
5. Thermodynamic calculations concerning the synthesis of pyridine, according to Nernst approximating formulae. Frames 960-964
6. The raffination effect of the liquid phase. Frames 965-969
7. Examination of DHD-catalysts prepared in the laboratory. Frames 970-978.