T. O. M. Microfilm Reel 031
(Original Identification reel 30AA)
Table of Contents
Note from the editors only selected documents from this microfilm reel have been completely processed and presented below in cleaned and grouped format (Bag 2170, Items 16, 20, and 23 only, identified by HTML links). The remainder of the reel is not related to the Fischer-Tropsch process, and therefore complete processing cannot be justified at this time.
We are, however, making the entire reel contents available in raw image format, although in a small number of relatively large files (rather than a very large number of small individual images). Anyone interested in pursuing the non-FT related material on this reel may find the document in these larger raw files.
Images 0001-0200 File size ca. 50 Mb
Images 0201-0400 File size ca. 44 Mb
Images 0401-0500 File size ca. 32 Mb
Images 0501-0600 File size ca. 67 Mb
Images 0601-0700 File size ca. 50 Mb
Images 0701-0800 File size ca. 46 Mb
Images 0801-0859 File size ca. 10 Mb
Bag 2170, Target 30/4.03 (?) I. G. Farben, Ludwigshafen
Continued from reel 030.
17. Chlorine production by HC1 oxydation Oppau process
18. Correspondence on polymerization at Rauxel
19. Experimental crotonaldehyde plant
21. Rikol
22. Correspondence on Renal process for producing hydrogen peroxide
24. Report on Hygas cracking processes of Koppers and I. G.
25. Studies on ultraviolet absorption (coronen and its derivatives), Raman spectra and other subjects at Ammoniaklaboratorium, Oppau.
Bag 2078, Target 30/4.03 Ludwigshafen
(a) Production and Engineering Data on the Manufacture of Butanediol and Butenediol
1. Summary of the heats of reaction for compounds entering into the Butadiene Synthesis.
2. Monthly Report of Diol separation and Butanediol Distillation Plant December 1944 and January 1945
3. Influence of diffusion on the reaction rate in Butenediol Hydrogenation
4. Report on the removal of silicic acid from the raw Butenediol Solution
5. Measurement of the concentration of Butanediol Solutions
6. Solubility of silicic acid in water, Butanediol and Butenediol
7. Average retention time of a carbon particle in the Butadiene Plant.
8. Heat of formation of Butenediol
9. First, Second, Third and Ninth Reports on Butenediol Manufacture
10. Monthly Report on Butanediol Manufacture
11. Monthly utility requirements for Betenediol, Butanediol and Butadiene production.
12. Distillation equipment in Lu 392
13. Visit to Dr. Steinhofer and Dr. Adam in Huls on May 20, 1943
14. Monthly Reports for October 1942 on Butadiene, Butenediol, Aldol Hydrogenation, Aldol Manufacture, Butenediol Hydrogenation, Butol Distillation, Aldehyde Manufacture and Catalyst Manufacture
15. Butadiene distillation at Schkopau.
16. The reaction Butenediol and Propargyl Alcohol with Alkalis
17. By-products of Butenediol Hydrogenation in the Reppe process
18. Use of Socol S for esterfying Colophonium
19. Testing of Socol DB as a Softening Agent for paper
20. Conference on the use of Butanediol bottoms as core oil
21 Excerpts from the record of the conference on Sucols of February 25, 1944.
22. Utilization of 1.4 Butanediol bottoms
23. Conference on Sucols February 25, 1944
24. Further discussion on Sucols conference, February 25, 1944
25. Results of experiments to determine the constitution of the lighter fractions of Butanediol bottoms
26. Letter giving properties and designations of the various Sucols
27. Memorandum on Core Oils
28. The constution of Asfluidols and Karboresins
29. Toxcity of Diols
30. Purity of technical Butanediol 1.4 for special purposes
31. Tests of a glycerine substitute
32. Glycerine substitute 5641
33. By-product from the Butanediol 1.4 distillation
34. Cutting oil
35. Plasticizer solution
36. Plasticizer for Polyamide
37. Method for obtaining 4-4 Dioxydibutyl Ether
38. Polyurethane
39. Production of polyurethanes from the residues of 1,4 Butanediol distillation
40. Polyurethane from Butanediol residues, testing of products
41. Utilization of 1.4 Butanediol bottoms
42. Testing of 4.4 Dioxydibutyl Ether as a glycerine substitute
43. Ammonium chloride for alkalin (core oil)
(b) Plant Design for Butanediol and Butenediol Manufacture
44. Plant data on Butanediol, etc.
45. Butanediol Plant Storage and Pumping Diagram
46. Flowsheet of Butanediol Hydrogenation
47. Impurities in acetylene in Month of May, 1943
48. Layout and construction details of Tetrahydrofuran Plant
49. Flowsheet of Tetrahydro Furan Plant
50. Chemical requirements Buna Manufacture
51. Cost estimate for the Butenediol Plant
52. Time schedule for starting up Ludwigshafen Buna Plant
53. Flowsheet for 1-3 Butol
54. Instrument flowsheet for Tetrahydro Furan
55. Flowsheet for hydrogenation of Butenediol
56. Building layout for Tetrahydro Furan Plant
57. Production and chemical consumption for Butanediol Plant 1943
58. Flowsheet for hydrogenation of Butanediol
59. Flowsheet for hydrogen purification
60. Hydrogenation flowsheet
61. General plan of hydrogen works
62. Instrument flowsheet
63. Flowsheet of Butadiene reactor section
64. Recovery of residues form Butanediol Manufacture
65. Material balance on Betanediol hydrogenation
66. Memorandum on Thermal Cracking of 1,3 Butanediol diacetate
67. Butadiene from mixtures of 1,3 and 1,.4 Butylene Glycol
68. Experiments on splitting water from 2 methyl Butanediol 1,3
(c) Flowsheets and drawings of Butadiene Manufacture
69. Table of flowsheet symbols
70. Tankage flowsheet for Butadiene manufacture
71. Flowsheet of Butadiene distillation. (Inert gas recovery system)
72. Flowsheet of Butadiene Distillation. (Wash tower and degasification)
73. Flow diagram for aldehyde destruction, pressure washing, and measuring vessels
74. Piping diagram (Operation No. 2)
75. Butadiene distillation (equipment layout)
76. Butadiene Plant building layout
77. Building layout continued
78. Flowsheet for butadiene distillation
79. Electrical heating circuit of Butadiene reactors
80. Apparatus and piping layout for Butadiene distillation refrigeration plant
81. Arrangement of entire Butadiene distillation
82. Flowsheet of Butadiene Reactor system
83. Butadiene Reactor System, Pipe and Instrument layout for high pressure steam system
84. Flowsheet for Butyraldehyde destruction
(d) Isobutylene Manufacture
85. Operating description of the ET 100 Plant (Isooctane)
86. Operating description of Isobutyl oil Distillation
87. Isobutyl oil distillation flowsheet
88. Separation of Methyl alcohol and Isobutyraldehyde
(e) Oxo Process, etc.
89. Production of Aldehydes in the Oxo Synthesis
90. Synthesis of Adipic Acid through the reaction of carbon monoxide on cyclic ethers, lactones, and diols
91. Synthesis of acetic acid through the reaction of carbon monoxide and methanol
92. Reaction of carbon monoxide with olefins and alcohols.
Continued on reel 032 Part I.