T.O.M. Microfilm Reel 028
(Original Identification Reel 28A)
Table of Contents
Note from the editors – only selected documents from this microfilm reel have been completely processed and presented below in cleaned and grouped format (Bag 2167, Section (j), and bag 2171 items 4 and 5 only, identified by HTML links). The remainder of the reel is not related to the Fischer-Tropsch process, and therefore complete processing cannot be justified at this time.
We are, however, making the entire reel contents available in raw image format, although in a small number of relatively large files (rather than a very large number of small individual images). Anyone interested in pursuing the non-FT related material on this reel may find the document in these larger raw files.
Images 0001-0100 File size ca. 52 Mb
Images 0101-0200 File size ca. 36 Mb
Images 0201-0400 File size ca. 44 Mb
Images 0401-0597 File size ca. 56 Mb
Bag 2077 Butol Manufacture (Butane-diol 1,3)
70. L-146301-2 Flowsheet
71. L-14631h-2 Flowsheet-high pressure steam
72. L-11879-4 Reactor details
73. L-6257-1 Distillation details
74. L-6127-1 Distillation details
75. L-6128-1 Distillation details
76. L-5540b-1 Distillation details
Butadiene Fractionation
77. Flowsheet
78. L-5936b-1 Distillation details
79. L-5937c-1 Distillation details
80. L-5938c-1 Distillation details
81. L-121586-4 Distillation details
Bag 2167, Target 30/4.03 – I. G. Farbenindustrie, Ludwigshafen
(a) Iso-octane from Isobutyl alcohol (Oppau)
1. N. 4186-4 Fractionation of raw isobutyl alcohol
2. Kd 1464 Flowsheet for fractionation of raw isobutyl alcohol
3. Kd 1848 Flowsheet for fractionation of raw isobutyl alcohol
4. Kd 539 Material balance for the manufacture of raw 50,000 tons per year of iso-octane
5. N 5395-4 Butyl alcohol fractionation
6. N 2640-1 Detail flowsheet for isobutyl alcohol fractionation, Part 1
7. N 2641-1 Same, Part 2
8. N 2427e-1 Same, Part 3
9. N 5321-8 Isobutyl alcohol fractionation Details column I
10. N. 5322-8 Same, column II
11. N 5323-8 Same, column Iia
12. N 5324-8 Same, column III
13. N 5325-8 Same, column IV
14. N 5326-8 Same, column V
15. N 5327-8 Same, column VI
16. BKOBS 1978-8 Isobutyl alcohol fractionation instrument details I
17. BKOBS 1978-8-a Same, Details II
18. ---- Material balance for 4000 tons per year of iso-octane
19. KD 2226 Proposed tankage
20. N 5533-2 Summary flowsheet for the manufacture of iso-octane from isobutyl alcohol
21. N 2607-1 Dehydrogenation of isobutyl alcohol, polymerization of isobutylene and depolymerization of tri-isobutylene
22. N 4903-4 Dehydration of isobutyl alcohol, 800 mm. diameter reactor
23. Kd 2209 Dehydration of isobutyl alcohol, 1300 mm. diameter reactor
24. Kd 2208 Flowsheet for the polymerization of isobutylene and fractionation of polymers
25. N 3707-4 Hydrogenation of di-isobutylene
26. N 6373b-2 Hydrogenation of di-isobutylene
27. N 12419-2 Hydrogenation of di-isobutylene
28. E 913-2 Hydrogenation of di-isobutylene (Electrical wiring diagram)
29. N 3462b-1 Hydrogenation of di-isobutylene – Piping Details
(b) Alternate Proposal for Iso-octane Manufacture (Oppau)
30. Material balance for the manufacture of iso-octane from mixed C4 hydrocarbons by chlorination
(c) Alkyl chloride Manufacture
31. N 10251-4 General flowsheet for alkyl chloride manufacture
32. N 10255-4 Prehydrogenation of propane
33. Flowsheet for alkyl chloride manufacture
34. N 5947-1 Detail flowsheet. Part I (chlorination)
35. Kd 1865 Proposed chlorination process
36. Kd 1880a Details of quarts illumination arrangement for chlorination
37. Kd 1903 Assembly of internal illuminating apparatus
38. N 5946-1 Detail flowsheet. Part II (distillation)
39. N 5948-1 Detail flowsheet. Part III
40. Kd 1871 Details of dehydrogenation apparatus
41. N 10253-4 Detail flowsheet. Part IV (fractionation after dehydrogenation)
42. N 5949-1 Detail flowsheet. Part V (removal of HC1)
43. N 13734-2 Plot plan of distillation
44. N13730-2 Plot plan of chlorination
45. N 13731-2 Plot plan of dehydrochlorination
46. N 13733-2 Plot plan of HC1 removal
47. Kd 1886a Plan of HC1 removal
48. Flowsheet for an alternate method of alkyl chloride manufacture (using propylene) Alky chloride from propylene. Alternate distillation method
(d) Butadiene Manufacture (Oppau)
50. P 282 Flowsheet for butadiene manufacture
51. P283 Material balance
52. N 8537-4 Material balance for the manufacture of butadiene, from butylene
53. Kd 454 Preliminary flowsheet for the chlorination of butylene
54. N 11801-2 Dehydrochlorination of dichlorobutane
55. Kd 1516 Butadiene washing and distillation
56. Kd 480 Flowsheet for butadiene distillation under pressure
57. Kd 523 Flowsheet for butadiene distillation with refrigeration
58. N 3686a-1 Plan and elevations for butadiene equipment
(e) Butadiene Polymerization (Oppau)
59. N 4202-8 Flowsheet for the manufacture of Buna D
60. N 7321-4 Flowsheet for the polymerization of butadiene
61. N 8218-4 Flowsheet for the polymerization of butadiene
62. Flowsheet for the polymerization of butadiene
(f) Manufacture of Oppanol (Oppau)
63. N 5278-2 Flowsheet of Oppanol plant
64. Kd 731 Details of polymerization reactors
65. N10387-4 Flowsheet for ethylene drying
66. Kd 1954 Piping for polymerization reactors
67. N11800-2 Flowsheet for ethylene refrigeration system
68. Kd 1003 Preparation of oppanol emulsion
69. Kd 1981 Preparation of oppanol emulsion
(g) Chlorine Recovery from HC1
70. Flowsheet for recovery of chlorine from HC1
71. Cl 129-4 Material balance flowsheet
72. Cl 106-2 Detail flowsheet – Part I
73. Cl 107-2 Detail flowsheet – Part II
74. Cl 108-2 Detail flowsheet – Part III
75. Cl 109-2 Detail flowsheet – Part IV
(h) Miscellaneous Chemicals
76. KV 308 Flowsheet for the manufacture of vinyl acetylene
77. Kd 1926a Flowsheet for the fractionation of ally alcohol
78. Flowsheet for the manufacture of formic acid
79. N9629-4 Flowsheet for the manufacture of formaldehyde
80. VASch 1001-8 Material balance for the manufacture of Vanol (ethylene glycol)
81. N12931-2 Flowsheet for the manufacture of Vanol
82. Material balance for the manufacture of diisopropyl ether
83. Kd 1855 Flowsheet for the manufacture of diisopropyl ether
84. B.Sk 68 Flowsheet for the manufacture of diisopropyl ether
85. N12883-2 Flowsheet for the manufacture of isoprene
86. Kd 2224 Flowsheet for the manufacture of pinicolin
87. Kd. 2233 Flowsheet for the purification of pinacolin
88. Kd 1452 Flowsheet for the manufacture of methacrylnitrite
89. Kd 1553 Material balance for the manufacture of crotonaldehyde
90. Kd 1551 Flowsheet for the manufacture of crotonaldehyde
(i) Crude Oil Refining (Oppau)
91. N 3841-2 General flowsheet of crude oil refining
(j) Synthetic Lube Oil from Ethylene
92. U 777-1 Detail flowsheet, Part I (Polymerization, catalyst separation). 1 page.
93. U 778-1 Detail flowsheet, Part II (AlCl3 complex decomposition). 2 pages.
94. U 779-1 Detail flowsheet, Part III (final oil refining and methanol recovery). 2 pages.
95. U 780-1 Detail flowsheet, Part IV (gas recovery). 2 pages.
96. U 791-1 Detail flowsheet, Part V (blending of ester oils and final clay treating). 2 pages.
(k) Iso-octane manufacture from Blechhammer & Brux feed stocks
97. Kd 1616 Material balance
98. Kd 1615 Material balance
99. Kd 1631 Butane isomerization
100. Proposed flowsheet for dehydrochlorination
101. Kd 1617 Proposed flowsheet for alkylation of Blechhammer stock
102. B.Sk 16 Alternate proposal for alkylation of Blechhammer stock
(l) Heydebreck Plant
103. N Flowsheet for products from isobutyl alcohol
104. N3989c-1 Isobutyl alcohol fractionation
105. N 9722-2 Flowsheet for the dehydrogenation of isobutyl alcohol
106. N9720a-2 Flowsheet for the fractionation of isobutylene
107. General flowsheet for chlorination operations
108. Kd2006b General flowsheet for the manufacture of 20,000 tons per year of isooctane
109. Kd 2034 Detailed flowsheet for the manufacture of isooctane, Part I
110. Kd 2033 Detail flowsheet for the manufacture of isooctane, Part II
111. Detail flowsheet for the manufacture of isooctane, Part III
112. Kd 2005 Flowsheet for the chlorination of isobutane (fractionation with gas oil wash in HC1 tower)
113. N. 10442-2 Flowsheet for the dehydrogenation of isobutyl chloride, polymerization if isobutylene, fractionation of polymers
114. U 440-16 Flowsheet for the isomerization of butane
115. Kd 2008a General flowsheet for the manufacture of 20,000 tons per year of butadiene
116. Kd 2055 Detail flowsheet for the manufacturing of butadiene, Part I.
117. Kd 2056 Detail flowsheet for the manufacture of butadiene, Part II
118. Flowsheet for the manufacture of ally chloride
119. Kd 2007a Material balance for propane dehydrogenation
120. Kd 1458 Methods of BF3 manufacture
121. Kd 1507 Flowsheet for the manufacture of BF3
122. N. 9721-2 Flowsheet for the manufacture of Oppanol
123. N 9719-2 Flowsheet for the liquefaction of ethylene
Bag 2171, Target 4.03 – I. G. Farbenindustrie – Ludwigshafen
1. Heide – Lube Oil Analysis
2. CO Removal (copper solution)
3. Alkylation, dehydrogenation, isomerization and exchange information
4. Methanization experiments (2 reports). December 2, 1942, and May 10, 1939. 18 pages.
6. Isooctane through chlorination, etc
73. Cl 107-2 Detail flowsheet – Part II
74. Cl 108-2 Detail flowsheet – Part III
75. Cl 109-2 Detail flowsheet – Part IV
(h) Miscellaneous Chemicals
76. KV 308 Flowsheet for the manufacture of vinyl acetylene
77. Kd 1926a Flowsheet for the fractionation of ally alcohol
78. Flowsheet for the manufacture of formic acid
79. N9629-4 Flowsheet for the manufacture of formaldehyde
80. VASch 1001-8 Material balance for the manufacture of Vanol (ethylene glycol)
81. N12931-2 Flowsheet for the manufacture of Vanol
82. Material balance for the manufacture of diisopropyl ether
83. Kd 1855 Flowsheet for the manufacture of diisopropyl ether
84. B.Sk 68 Flowsheet for the manufacture of diisopropyl ether
85. N12883-2 Flowsheet for the manufacture of isoprene
86. Kd 2224 Flowsheet for the manufacture of pinicolin
87. Kd. 2233 Flowsheet for the purification of pinacolin
88. Kd 1452 Flowsheet for the manufacture of methacrylnitrite
89. Kd 1553 Material balance for the manufacture of crotonaldehyde
90. Kd 1551 Flowsheet for the manufacture of crotonaldehyde
(i) Crude Oil Refining (Oppau)
91. N 3841-2 General flowsheet of crude oil refining
(j) Synthetic Lube Oil from Ethylene
92. U 777-1 Detail flowsheet, Part I (Polymerization, catalyst separation). 1 page.
93. U 778-1 Detail flowsheet, Part II (AlCl3 complex decomposition). 2 pages.
94. U 779-1 Detail flowsheet, Part III (final oil refining and methanol recovery). 2 pages.
95. U 780-1 Detail flowsheet, Part IV (gas recovery). 2 pages.
96. U 791-1 Detail flowsheet, Part V (blending of ester oils and final clay treating). 2 pages.
(k) Iso-octane manufacture from Blechhammer & Brux feed stocks
97. Kd 1616 Material balance
98. Kd 1615 Material balance
99. Kd 1631 Butane isomerization
100. Proposed flowsheet for dehydrochlorination
101. Kd 1617 Proposed flowsheet for alkylation of Blechhammer stock
102. B.Sk 16 Alternate proposal for alkylation of Blechhammer stock
(l) Heydebreck Plant
103. N Flowsheet for products from isobutyl alcohol
104. N3989c-1 Isobutyl alcohol fractionation
105. N 9722-2 Flowsheet for the dehydrogenation of isobutyl alcohol
106. N9720a-2 Flowsheet for the fractionation of isobutylene
107. General flowsheet for chlorination operations
108. Kd2006b General flowsheet for the manufacture of 20,000 tons per year of isooctane
109. Kd 2034 Detailed flowsheet for the manufacture of isooctane, Part I
110. Kd 2033 Detail flowsheet for the manufacture of isooctane, Part II
111. Detail flowsheet for the manufacture of isooctane, Part III
112. Kd 2005 Flowsheet for the chlorination of isobutane (fractionation with gas oil wash in HC1 tower)
113. N. 10442-2 Flowsheet for the dehydrogenation of isobutyl chloride, polymerization if isobutylene, fractionation of polymers
114. U 440-16 Flowsheet for the isomerization of butane
115. Kd 2008a General flowsheet for the manufacture of 20,000 tons per year of butadiene
116. Kd 2055 Detail flowsheet for the manufacturing of butadiene, Part I.
117. Kd 2056 Detail flowsheet for the manufacture of butadiene, Part II
118. Flowsheet for the manufacture of ally chloride
119. Kd 2007a Material balance for propane dehydrogenation
120. Kd 1458 Methods of BF3 manufacture
121. Kd 1507 Flowsheet for the manufacture of BF3
122. N. 9721-2 Flowsheet for the manufacture of Oppanol
123. N 9719-2 Flowsheet for the liquefaction of ethylene
Bag 2171, Target 4.03 – I. G. Farbenindustrie – Ludwigshafen
1. Heide – Lube Oil Analysis
2. CO Removal (copper solution)
3. Alkylation, dehydrogenation, isomerization and exchange information
4. Methanization experiments (2 reports). December 2, 1942, and May 10, 1939. 18 pages.
5. Miscellaneous Invention (Patent) Disclosures – covering a wide variety of hydrocarbon processing related topics. Includes a number of disclosures on aspects of the Fischer-Tropsch synthesis. 75 pages.
6. Isooctane through chlorination, etc