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T. O. M. Microfilm Reel No. 009

(Originally Roll 9A)

 

Table of Contents

 

 

Note from the editors – only selected documents from this microfilm reel have been completely processed and presented below in cleaned and grouped format (Item 15 only, identified by HTML links).  The remainder of the reel is not related to the Fischer-Tropsch process, and therefore complete processing cannot be justified at this time.

 

We are, however, making the entire reel contents available in raw image format, although in a small number of relatively large files (rather than a very large number of small individual images).  Anyone interested in pursuing the non-FT related material on this reel may find the document in these larger raw files.

 

                                                Images 0001-0200                   File size ca. 30 Mb

                                                Images 0201-0400                   File size ca. 40 Mb

                                                Images 0401-0600                   File size ca. 19 Mb

                                                Images 0601-0800                   File size ca. 20 Mb

                                                Images 0800-0970                   File size ca. 15 Mb

 

 

 

Bag 2733 Target #30/4.11-Bottrop.

 

                                                                                                                                                               

ITEM:                                                                                                                                                                    

 

6.  Naptha Refining:  Memoranda with tables and graphs showing fractionation  and separation of components of tar residue.  Fractions        were treated with sulfuric acid.  Colored substances and some pyridine were isolated.  Comments on and tables of plant samples of aviation gasoline received from Gelsenberg-Benzin AG, from Scholven-Benzin CV and from Technikum-Benzin from Catalyst 7019 during 1940.  1939-44.  49 pages.

 

7. Pitch Compartment Balance Sheets:  Chlorine determination balances of operating plant by months.  1942-44.  30 pages.

 

8. Pitch Compartment Balance Sheets:  Monthly summary tables showing time in operation, throughput; products in terms of (1) stripped oil (2) tar (3) water (4) salts of ammonia, carbon dioxide, hydrogen sulfide and phenol;  hydrogen gas, hydrocarbon gases through C5.  April 1938 – June 1944.  95 pages.

 

9. Vapor Phase Balance Sheets:  Same from June 1939 to June 1944 with special summary showing calculated distribution of products when running to three different percentages of fuel oil production.  74 pages.

 

10. Miscellaneous Information at 700 Atmospheres: 

(a)  Minutes of conference on gas hydrates held on Dec. 4, 1941, at Ludwigshafen.  List of 45 names in attendance, few

sketches, graphs, literature references.  50 pages.

(b)  Miscellaneous communications on other conferences, gas-holders, compressors, gas hydrates, corrosion.  February

1941-1945.  80 pages.

(c)  Dr. Matthias Pier’s 60th birthday, July 1942.  He was director of high pressure work for Farbenindustrie.  4 pages                    (d)  Miscellaneous annalytical methods.         1938-40.  24 pages.

(e)  Calcium ferricyanide to determine H2S.  1943-44.  10 pages.

(f)  Report on explosion of gasholders.                  1943-44.  9 pages.

 

11. Yields and Balances:  Ammonia, hydrogen sulfide and sulfur, miscellaneous reports.  1938-44.  12 pages.

 

12. Plant Extraction Balances: By months.  1942-44.  77 pages.

 

13.  Laboratory Analyses of Gases, Oils and Solid Extractions:  Plant Operation  1941-42.  35 pages.

 

14.  Erection Costs, etc.

(a)            Three secret letters dated Dec. ’44 and Jan ’45, proposing to build a high pressure hydrogenation plant in

                a chalk pit in a valley near Sargard on the Rguen to protect it from aircraft.  16 pages.

(b)                 Letter on hot separation under 700 atmospheres.  20 Feb. 1945.  2 pages.

(c)            Letter on regeneration of middle oil under high pressure in soecial gas chamber.  24 Aug. 1943.  4 pages.

(d)           Tabulated costs of erection of regeneration chamber.  2 pages.

(e)              Flow diagrams, sketches, charts, equipment costs, product costs, etc. for solid extractions and electrode coke.                 1941-43.  70 pages.

 

15. Analytical Methods Fischer-Tropsch, Ruhrchemie:  Analytical methods with complete six page index for analyzing motor  fuels prepared according to the Ruhrchemie-Fischer-Tropsch process.  100 pages.

 

16. Experimental – General:  Memoranda on following subjects:

Corosion middle oil and phenols                            1942        4

Explosibility of oil-air mixtures                              1942        3

Solvents                                                                  1942        2

Polymerization of gas oil and ethylene                                   6

 

17. Liquid Phase – Experimental: Charts showing % of products in research experiments, not dated.  13 pages.

                                               

18. Experiments Filtration: Memoranda on filtering experiments.  1937-42.  7 pages

 

19. Experiments Extraction: Most in 1938.  Few 1940.  110 pages.

 

20. Bottrop Analytical

(a)      Loose Leaf Analytical Manual of the head laboratory, Welheim containing methods used by the Teerzeugnusse GmbH, Essen.  49 pages.

(b)   Pamphlet entitled “Organic Metal Reagents” by E. Merk of Darmstadt.  Copy belonging to the head laboratory of 

       Ruhrol GmbH, Hugo Stinnes Works.  30 pages.