|
9:30 |
The Development and application of Planning Processes to meet environmental restoration and waste management data needs. |
6 |
|
9:50 |
DOE’s quality assessment program for environmental restoration and waste management (EM) sampling and analysis activities |
7 |
|
10:40 |
Fifty Years of continuous improvement. (What has DOE done for analytical chemistry?) |
9 |
|
11:00 |
Titrimetry and spectrophotometry: from colors to computers. |
10 |
|
11:20 |
Evolution of Plutonium measurements at lanl. |
11 |
|
11:40 |
From Hevesey to the advanced neutron source – the past and final frontier of neutron activation analyses. |
12 |
|
1:30 |
Prediction of chemical properties of organic compounds from Molecular structure. |
14 |
|
1:50 |
The Nist Consortium on Automated analytical laboratory systems. |
15 |
|
2:10 |
Status of the contaminant analysis automation (CAA) Program. |
16 |
|
2:30 |
From liquid sample to printed report: A fully automated plutonium analyzer. |
17 |
|
3:20 |
Automated test apparatus for the modeling of VOC transport in lab-scale simulated waste Drums |
18 |
|
3:40 |
Multi-media analytical procedures, sound, graphics, video clips in procedures. |
19 |
|
4:00 |
Implementation of a laboratory information management system for environmental regulatory driven analyses. |
20 |
|
Wednesday, AM October 6, 1993 - Electroscopy ionization – Mass Spectrometry |
22 |
|
8:30 |
An overview of electroscopy ionization-mass spectroscopy. |
22 |
|
9:10 |
The roles of colvation and surface chemistry in ion desorption. |
24 |
|
10:10 |
Probing covalent protein adducts by means of electrospray |
|
|
10:40 |
High resolution precision mass measurements of biopolymers by electrospray ionization Fourier transform iron cyclotron resonance mass spectrometry. |
26 |
|
11:10 |
Chemical derivatization for selective detection by electroscopy mass spectrometry |
27 |
|
Wednesday, PM: Detection and Monitoring of Airborne Toxics |
28 |
|
1:30 |
Overview of optical remote sensing for detection of air toxics. |
28 |
|
1:50 |
Air Issues during site remediations: Regulatory considerations and case study |
29 |
|
2:10 |
Development of analytical methods for toxic byproducts in gases from soil remediation systems. |
30 |
|
2:30 |
Air Quality monitoring by Membrane sampling ion trap mass spectrometry. |
31 |
|
2:50 |
Evaluation of FTIR spectroscopy for the analysis of waste drum headspace. |
32 |
|
3:10 |
Is the sampling of drum headspace VOCs aviable waste characterization tool? |
33 |
|
Wednesday PM: Laboratory management and quality assurance |
35 |
|
1:30 |
Performance Avaluation programs alternatives based on user needs. |
35 |
|
1:50 |
A quality assessment program as a tool for improving analytical laboratory performance. |
37 |
|
2:10 |
TQM success in the analytical laboratory. |
39 |
|
2:30 |
Uncertainty in analytical measurements. |
40 |
|
2:50 |
Validation of NAA of environmental samples |
41 |
|
3:10 |
Quality assurance in environmental management. |
42 |
|
|
Microwave sample preparation for cold vapor atomic absorption spectrosmetry |
48 |
|
|
Experimental and theoretical relative ion yields for glow discharge Mass Spectrometry. |
49 |
|
|
Secondary ion and ms/ms images of biological samples. |
54 |
|
|
The determination of tnt and tnt degradation products in soil by HPLC and other analytical methods. |
55 |
|
Wednesday PM: Interactive Analytical Seminars |
44 |
|
3:40-5:00 |
Nuclear waste analytical reound robins 1-6: Lessions learned. |
44 |
|
|
Calibration and use of Cf shufflers for analyzing waste drums. |
46 |
|
|
Estimating analytical laboratory capacity. |
47 |
|
|
Analysis of fluoride in molten salt mixtures using microwave digestion. |
51 |
|
|
Direct analysis of oils by solution residue glow discharge mass spectrometry |
52 |
|
|
Determination of relative sensitivity factors for the quantitative analyses of clays by glow discharge mass spectrometry. |
53 |
|
|
Detection of cyclohexylamine on laboratory and environmental surfaces using static sims. |
57 |
|
|
Separation of actinide elements in environmental samples. |
58 |
|
|
Determination of radionuclides in soils and waters by ICP-MS using flow-Injection concentration and ultrasonic nebulization. |
59 |
|
|
Direct and simultaneous determination and quantification of radium-226 and radium-228 by liquid scintillation counting. |
60 |
|
|
Tru-Spec and re-spec chromatography basic studies and applications. |
61 |
|
|
On-line mercury in water monitor. |
62 |
|
|
Elements of benchtop quality control. |
63 |
|
|
New techniques for improving icp-oes sample throughput. |
64 |
|
|
How we developed a data validation program. |
65 |
|
|
Radioactive sample analysis by ICP/MS. |
66 |
|
|
Lasers and ion traps. |
67 |
|
|
Microscale liquid phase sensors: Chromatography on a chip. |
68 |
|
|
Diode laser spectroscopy for practical isotope ratio measurements. |
69 |
|
|
Determination of oil and Grease in wastewater by solid-phase extraction. |
70 |
|
|
Improving method for the determination of actinide elements in soils. |
71 |
|
|
DOE Methods for evaluating environmental and waste management samples: New Methods. |
73 |
|
|
Methods for sampling wastes and environmental media at DOE sites. |
75 |
|
|
The determination of 230th in soils by laser ablation ICP-Mass spectrometry. |
76 |
|
|
Neutron activation analysis for large-scale environmental studies. |
77 |
|
|
Automation of a Gamma Ray Spectroscopy system using laboratory robotics. |
78 |
|
|
Maximizing the cold neutron flux from a californium-252 source. |
79 |
|
|
A comparison of extraction of soils using the toxicity characteristic leaching procedure and total metal metal digestion. |
80 |
|
|
Characterization of Hepa for disposal. |
81 |
|
|
Radiostrontium analysis using combined cation exchange-extrication media methods. |
82 |
|
|
Managing a subcontract laboratory |
83 |
|
|
Laser mass spectrometry for oligonucleotide analysis. |
84 |
|
|
Nondestructive measurement of combustible waste containing uranium in a B-25 box. |
85 |
|
|
High Speed separations to measure impurities in PU-238 oxide and trace R Dionuclides in High Activity waste at SRS. |
86 |
|
|
High speed column removal of radioactive cesium and strontium to lower exposure during analysis of high activity waste at SRS. |
87 |
|
|
Integration of mobile laboratories into an analytical service strategy for environmental restoration. |
88 |
|
|
Applications of extraction chromatography in radiochemical analyses. |
89 |
|
|
Terratrog soil/water gas sampling system. |
90 |
|
Thursday AM: Waste and environmental sampling |
92 |
|
8:30 |
Opening remarks. |
92 |
|
8:40 |
Measurement and spatial modeling of VOC contamination in soils. |
92 |
|
9:05 |
Development of sampling techniques for inel stored TRU solidified/stabilized waste forms |
94 |
|
9:30 |
Establishment of multiple phase sampling capability for characterization of nuclear wastes. |
95 |
|
9:55 |
Drilling and sampling methodology for the collection of highly radioactive soil samples. |
96 |
|
10:35 |
In SITU Characterization: The next generation. |
98 |
|
11:00 |
Rapid isolation and measurement of TC-99. |
99 |
|
11:25 |
Analysis and verification of compressed gas cylinders. |
100 |
