I |
Abstract |
1 |
II |
Objective |
2 |
III |
Summary of Progress |
4 |
IV |
Detailed Description of Technical Progress |
7 |
|
1 |
Task 1 - Project Work Plan |
7 |
2 |
Task 2 - Slurry Catalyst Development |
7 |
|
2.1 |
Catalyst Preparation and Characterization |
7 |
|
2.1.1 |
Catalyst Preparation |
7 |
2.1.2 |
Co-Precipitation Procedure |
8 |
2.1.3 |
Impregnation Procedure |
9 |
2.1.4 |
Catalyst Characterization |
10 |
2.2 |
Product Analysis System |
13 |
|
2.2.1 |
Carle AGC 400 Modifications |
13 |
2.2.2 |
Response Factors for the Organic Phase Components |
13 |
2.3 |
Data Acquisition and Reduction |
15 |
|
2.3.1 |
Anderson-Schulz-Flory (ASF) Plotting Programs |
15 |
2.3.2 |
Peak Identification Software |
16 |
2.4 |
Design and Construction of Reactor Systems |
19 |
|
2.4.1 |
Catalyst Reduction Unit |
19 |
2.4.2 |
Fixed Bed Reactor Apparatus |
20 |
2.4.3 |
Slurry Bed Reactor Apparatus |
20 |
2.5 |
Testing of the Existing Slurry Reactor System |
21 |
|
2.5.1 |
Blank Runs |
21 |
2.5.2 |
Wax Withdrawal Experiments |
22 |
2.5.3 |
Catalyst Separation from Slurry Samples |
23 |
2.6 |
Shakedown Runs with a Fused Iron Catalyst |
24 |
|
2.6.1 |
Catalyst Activation |
24 |
2.6.2 |
Shakedown Run in the Slurry Reactor |
26 |
2.6.3 |
Shakedown Run in the Fixed Bed Reactor |
30 |
3 |
Task 3 - Process Evaluation Research |
35 |
V |
Literature References |
36 |
|
Tables |
38 |
Figures |
54 |
App. I |
Sample Output of the Mass Balance Program (Run
SA-01-0817-5) |
75 |