TITLE: Separation of Fischer-Tropsch wax from catalyst by supercritical fluid extraction. Technical progress report, January--March 1995. AUTHOR: M. C. Thies. INST. AUTHOR: Clemson Univ., SC. Dept. of Chemical Engineering. SPONSOR: Department of Energy, Washington, DC. LANGUAGE: English PUB. TYPE: Technical Report PUB. COUNTRY: United States SOURCE: Department of Energy [DE], 1995, 3p. NTIS ORDER NO.: DE95015610INW ABSTRACT: Objective is to evaluate the potential of supercritical fluid extraction for separating the catalyst slurry of a Fischer-Tropsch (F- T) slurry bubble column reactor into a wax and a concentrated catalyst slurry that is ready for recycle/regeneration. The automated apparatus was evaluated using a toluene-petroleum pitch system. The Statistical Associating Fluid Theory (SAFT) equation will be used to fit the VLE and LLE data for F-T wax-solvent systems; this equation was successful in predicting both phase compositions and average molecular weight distributions. REPORT NUMBER: DOE/PC/94219-T2 CONTRACT NUMBER: FG22-94PC94219 |