TITLE: Advance concepts for conversion of syngas to liquids. Quarterly report, September 28, 1994--January 28, 1995.

AUTHOR: R. Szostak;   G. Abotsi;   M. Mitchell;   C. Ingram.

INST.  AUTHOR: Clark Atlanta Univ., GA.

SPONSOR: Department of Energy, Washington, DC.

LANGUAGE: English

PUB.  TYPE: Technical Report

PUB.  COUNTRY: United States

SOURCE: Department of Energy [DE],  1995,  16p.

NTIS ORDER NO.: DE96000918INW

ABSTRACT:

In this study, MeAPO-36 was crystallized from a reaction mixture of molar composition 1.8 Pr(sub 3)N; 0.156 MgO; 0.97 Al(sub 2)O(sub 3); 0.936 P(sub 2)O(sub 5); 41.4H(sub 2)O; and 0.31 HOAC at 100 C for 48 h followed by 150 C for 24 to 72 h. Its formation was dependent on the source of aluminum, template concentration and the reaction temperature and time. MeAPO-5 was a competing impurity phase and its formation can be suppressed by changes in the reaction conditions. The report includes a discussion of the synthesis procedure for MeAPO-36 and its characterization by x-ray diffraction.

REPORT  NUMBER: DOE/MT/94010-T1

CONTRACT  NUMBER: FG22-94MT94010