TITLE: Technology development for iron Fischer-Tropsch catalysts. Quarterly technical progress report period ending June 30, 1991. AUTHOR: B. H. Davis. INST. AUTHOR: Kentucky Univ. Research Foundation, Lexington. SPONSOR: Department of Energy, Washington, DC. LANGUAGE: English PUB. TYPE: Technical Report PUB. COUNTRY: United States SOURCE: Department of Energy [DE], 1991, 29p. NTIS ORDER NO.: DE92013923INW ABSTRACT: A number of (alpha)-FeOOH samples were prepared at differential experimental conditions and characterized by X-ray diffraction, surface area, and TEM. Precipitation of ferrous hydroxide and subsequent oxidation will produce (alpha)-FeOOH, Fe(sub 3)O(sub 4), (gamma)-FeOOH or (delta)-FeOOH depending on the experimental conditions such as (Fe)/(OH) ratio, starting iron compound, precipitation/oxidation temperature, oxidizing agent, aging, and modifiers. In the present study we have carried out experiments on the effect of (Fe)/(OH) ratio as well as the oxidizing agent on the nature of final oxidized iron compound. REPORT NUMBER: DOE/PC/90056-T3 CONTRACT NUMBER: AC22-91PC90056 |