TITLE: Development of precipitated iron Fischer-Tropsch catalysts. Quarterly technical progress report, October 1, 1994--December 31, 1994. AUTHOR: D. B. Bukur. INST. AUTHOR: Texas A and M Univ., College Station. Dept. of Chemical Engineering. SPONSOR: Department of Energy, Washington, DC. LANGUAGE: English PUB. TYPE: Technical Report PUB. COUNTRY: United States SOURCE: Department of Energy [DE], 1 Mar 95, 15p. NTIS ORDER NO.: DE95009334INW ABSTRACT: The work on Task 3. Testing of Previously Synthesized Catalysts was initiated in early October as scheduled. Two initial tests were not successful (runs SB-2764 and SB-3064). It took us a great deal of time and effort to overcome these problems, which included conducting a blank test (run SB-3184) and a test of commercial Ruhrchemie catalyst (run SB-3254). Finally, a successful test of catalyst with nominal composition 100 Fe/5 Cu/6 K/24 SiO(sub 2) (run SB-3354) was completed using a different slurry medium (Ethylflo 164 oil). Low activities in unsuccessful tests SB-2764 and SB-3064 may be due to catalyst poisoning by impurities in the initial slurry medium (purified n-octacosane from Humphrey Chemical Co.). REPORT NUMBER: DOE/PC/93069-3 CONTRACT NUMBER: AC22-94PC93069 |