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T.A.C. REPORT ZAL-1
ANALYTICAL METHOD REPORT No. 1

TABLE OF CONTENTS

Page No.
Section 1
421 kb

Cover Page

Table of Contents
Section 2
1139 kb
I. Summary 1
II. Introduction 3
III. Personnel Interviews 3
IV. Plant and Laboratory Visits 5
V. Documents 6
VI. Abstracts of Analytical Reports from Oppau, Ludwigshafen, and Leuna
1. Analytical determination of ammonia, mono-, di-, and trimethylamine, Leuna, September 30, 1932 6
2. Research on the determination of impurities in electric are acetylene by fractional distillation, Leuna, December 29, 1933 7
3. Analytical determination of gas mixtures, in particular those containing  large amounts of gaseous hydrocarbons, Leuna, April 5, 1933 7
4. Volumetric determination of two olefin groups. Leuna, March 28, 1939 9
Section 3
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5. Quantitative determination of low boiling point phenols in phenolic oils by close fractionation 10
6. Report on a conference on molecular spectra held in Leuna on January 21, 1941 10
7. Isoprene determination. Leuna, December 30, 1943. 11
8. Research with a new indicator to replace Methyl Orange. Leuna, December 7, 1936 12
9. Determination of bromide number in benzines and other olefinic solutions. Leuna 12
10. New infrared method for gas analysis.  Oppau, May 10, 1938 13
11. Researches with the electron microscope.  Oppau, June 6, 1936 13
12. Determination of nitrogen in coals, tars, oils, benzines, and similar products.  Analytical laboratory.  Oppau, Ocober 10, 1938 14
13. The determination of Phosgene, Thionylchloride, Sulfurous Acid, Chlorine, and Sulfur Dichloride in the presence of each other. Ludwigshafen, May 2, 1943 15
14. Research on Benzines of high olefin content, particularly on determination of the aromatic content. Oppau, June 1, 1939 17
15. Determination of acetylene and hydrocarbons in liquid oxygen from the Linde apparatus. Leuna, May, 1940 19
16. The determination of olefins and aromatics in hydrocarbon mixtures. Oppau, April 7, 1941 21
17. Volumetric determination of very small amounts of sulfur in benzines, phenols, and leaves. Leuna, April 10, 1941 22
18. Fluorine and silicic acid determination in cryolite. Leuna, March 8, 1941 22
19. Determination of sulfate in sulfonated detergents and wetting agents. Leuna, December 4, 1941 23
20. Research on phosphoric acid determination in catalysts. Leuna, May 8, 1941 23
21. A new method for the oxidation splitting of ozonides. Leuna, June 11, 1941 24
22. Potentiometric molybdenum titration. Leuna, June 30, 1936 25
23. Determination of available sulfur in polysulfide solutions. Leuna, February 7, 1941 26
Section 4
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24. Measure of the reaction heat of the condensation of an aliphatic aldehyde. Leuna, February 10, 1941 27
25. Preparation, properties, and comparative capillary chemistry research on eight sulfonates and sulfates derived from hexadecane. Leuna, January, 1941 27
26. Volumetry of non-ideal gases.  More volume of butadine. Leuna, March, 1939 29
27. Comparison of various procedures for the determination of olefins. Leuna, February 15, 1943 29
28. The ultraviolet colorimeter, a control apparatus for the determination of phenol and other substances. Leuna, October 2, 1941 30
29. Analytical methods for Mersol, Mersolate, and wetting agents containing Mersolates. Further developments in 1942. Leuna, January 27, 1943 30
30. Determination of minute amounts of carbon disulfide. Leuna, February 1, 1943 31
31. Separation of the di- and polysulfochlorides in Mersol by precipitation with hydrocarbons. Leuna, February 1, 1943 32
32. Volatility of H2S in solution of various hydrogen ion concentrations. Leuna, November 18, 1929 33
33. The preparation of methoxylbutadiene from crotonaldehyde acetylization products. Leuna, May 14, 1942. 33
34. Methods and apparatus for the determination of water vapor in gases by means of calcium nitride Ludwigshafen, February 7, 1942 33
35. The physical-chemical principles of extinction spectrography and its uses in visible and long wave ultraviolet light. Leuna, October 3, 1942 35

. 36 Efficiency of laboratory columns. Leuna, December 5, 1940 35
Section 5
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37. On the nature of the aromatic hydrocarbons present in prehydrogenation products. Leuna, April, 1931 36
38. Quantitative determination of ethylene oxide. Oppau, January 31, 1938 36
39. The vacuum rectification of the mixture phenetolbenzylamine in empty glass tubes. Leuna, October 23, 1944 37
40. Volumetric analyses with iron salts. (Ferrometry). Leuna, December, 1941 38
41. Investigation of ketone oils. Leuna, February 23, 1943 39
42. Investigation on the nature of the higher boiling half of the xylenol fraction of the M-phenolic oil. Leuna, October 12, 1942 41
43. Investigation of the K-fraction. Leuna, February 23, 1943 41
44. Determination of benzoyl peroxide. Leuna, April 29, 1942 42
45. Patent Application. Frankfurt am Main, March 18, 1940. Procedure for the separation of aliphatic oxygenated compounds, as well as straight chain hydrocarbons containing at least 6 carbon atoms, from mixtures containing these compounds 43
. 46 Analytical and preparative accurate separation of hydrocarbon mixtures. Oppau, March 14, 1930 43