PATENTS
Spent catalyst containing Th is treated with a mineral acid to dissolve the Th and, if desired, the other catalyst constituents. A sludge is precipitated by Na2CO3 from the acid solution obtained. This sludge contains a large amount of Th. The sludge is dissolved in H2SO4. The Th is precipitated by K2SO4 from the H2SO4 solution obtained as Th-K sulfate, which in turn is separated from the solution. An insoluble Th (CO3)2 is prepared from the sulfate and the carbonate is recovered. |