3306. STRIMBECK, G. R., HOLDEN, J. H., ROCKENBACK, L. P., CORDINER, J. B., AND SCHMIDT, L. D. Pilot-Plant Gasification of Pulverized Coal With Oxygen and Highly Superheated Steam. Bureau of Mines Rept. of Investigations 4733, 1950, 41 pp.; Bib. of Tech. Repts., vol. 15, 1951, p. 43; PB 101,855; Proc. Am. Gas Assoc., 1950, pp. 501-563. Pilot-Plant data are reported for 31 runs on the gasification of 90% through 200-mesh of a strongly coking Sewickley-bed coal with O2 and with superheated steam in 3 temperature ranges 2,700°-3,400° F., 1,600°-2,000° F., and 230°-250° F., at feed rates of 200-450 lb. per hr. Average requirements per 1,000 std. cu. ft. of CO+H2 produced are:
In general, the pilot plant performed very well. Continuous operation was possible, the runs being terminated voluntarily. The performance data indicate that the process could furnish low-cost synthesis gas on a commercial scale. The % gasification of the coal was very satisfactory. Average % C gasified was 8.9, 89.9, and 85.2 in the high-, medium-, and low-temperature steam runs, respectively. The O2 requirement per 1,000 std. cu. ft. of CO+H2 produced in the high-temperature steam runs was lower than for any other continuous process known. Correlations re presented on steam decomposition, O2 required per 1,000 cu. ft. of CO+H2 in the make gas, % CO2, and H2:CO ratio in the make gas. Refractory materials suitable for use in superheating steam to the range of 2,700°-3,400° F. have been found to be available at a reasonable cost. Apparatus is described with the aid of flow diagrams.
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