2645. ---------------. [PETROLEUM PROCESSING.] Gas-Synthesis Plant. Vol. 5, No. 9, 1950, pp. 946-947. Major construction work has been completed on the Bureau of Mines gas-synthesis demonstration plant at Louisiana, Mo., which will convert coal into liquid fuels by a modified Fischer-Tropsch process. The plant, of 80-100-bbl. per day capacity, was built at a cost of $4,915,000. It is expected to begin integrated operations early next year. Modifications of the German Fischer-Tropsch process include improvements in the method of producing and purifying the synthesis gas, the use of a rugged, granular, synthetic-NH3 type Fe catalyst, and the use of a fluidized-bed, internally cooled converter. The synthesis gas will be obtained by gasifying pulverized coal ranging from anthracite to lignite with O2 and superheated steam. O2 for the process will be extracted from the air at temperatures of more than 300° F. below zero in a Linde-Fränkl unit; it will be 98% pure. The gasification unit is briefly described. It will use about 28 tons of coal, 24 of O2, and 35 of superheated steam to produce 2,000,000 ft.3 of raw synthesis gas daily. It is already demonstrated that a gas of normal composition (41% CO, 38% H2, 16% CO2, and 5% N2 and impurities) can be produced. As an auxiliary source of synthesis gas, a 7-ft.-diameter Kerpely producer modified to operate continuously with coke and O2 has been installed. Anticipated daily production will be 55-60 bbl. of 75-octane gasoline, 10-12 bbl. of 80-octane diesel oil, and about 12 bbl. of heavy oils and waxes suitable for cracking stock. Process-flow diagram of the plant is shown. |