2474. ---------------. [NIKITIN, V. M.] [Treatment of the Byproducts From the Methanol Synthesis. III.] Jour. Chem. Ind. (U.S.S.R.), vol. 14, 1937, pp. 993-996; Chem. Abs., vol. 32, 1938, p. 1647. Isobutyl acetate prepared from the iso-BuOH in synthetic MeOH can be dried by neutralizing with Na2CO3 and distilling into a continuous separator, or dried over CaSO4. The higher-boiling oil from the MeOH is best-dried by salting out the NaCl and drying over CaO or CaSO4. |