T.O.M. Microfilm Reel 252

(Original Designation BM-38)

Table of Contents

Note from the editors - only selected documents from this microfilm reel have been completely processed and presented below in cleaned and grouped format (Section XI item only, identified by HTML link below). The remainder of the reel is not related to the Fischer-Tropsch process, and therefore complete processing cannot be justified at this time.

We are, however, making the entire reel contents available in raw image format, although in a small number of relatively large files (rather than a very large number of small individual images). Anyone interested in pursuing the non-FT related material on this reel may find the document in these larger raw files.

Images 0001-0046 File size ca. 17 Mb

Images 0119-0200 File size ca. 32 Mb

Images 0201-0300 File size ca. 37 Mb

Images 0301-0400 File size ca. 36 Mb

Images 0401-0500 File size ca. 39 Mb

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Images 0901-0977 File size ca. 27 Mb

Index to microfilm of Dr. Pier’s files

IX. Diesel Oil.

ITEM NO.

1. Higher flash point Diesel oil. Frames 1-11

X. Economics.

2. Cost of aviation gasoline from pitch. Complete cost breakdown. Frames 12-28

2a. Estimates of costs of aviation gasoline from Rumanian oil in Politz. Frames 29-37

XI. Fischer-Tropsch.

1. State of the synol process in June 1941. By Michael. June 24, 1941. Frames 38-42. 5 pages.

2. Synthesis with iron catalysts. By Peters. June 24, 1941. Frames 43-44. 2 pages.

3. Patent for production of hydrocarbon fluids from gaseous carbon compounds. No number or date. Frames 45-49. 10 pages.

6. Organic materials in the product liquor of the foam process. By Schmidt and Michael. February 22, 1943. Frames 50-51. 2 pages.

7. Equilibria in Fischer-Tropsch. By Schneider. May 5, 1943. Frames 52-53. 2 pages.

8. Operating report of a 1.5 m³ plate foam converter in the Fischer-Tropsch process. By Michael. July 3, 1942. Frames 54-59. 6 pages.

9. The alcohol synthesis. Discussion. By Michael. July 11, 1941. Frames 60-62. 3 pages.

10. Running the synthesis products to alcohols, fatty acids, and sulfonates. By Michael. June 19, 1942. Frames 63-64. 2 pages.

11. The state of the Fischer-Tropsch synthesis, July 1941. By Michael. July 24, 1941. Frames 65-82. 19 pages.

13. Replacing cobalt by iron. By Michael, et al. April 19, 1943. Frames 83-90. 8 pages.

14. State of synthesis oil research. June 10, 1941. Frames 91-93. 3 pages.

15. Alcohol synthesis from CO:H₂ by means of the hot gas recirculation process. By Michael. September 13, 1941. Frames 94-97. 4 pages.

18. State of synthesis oil research. Alcohol process; olefin process; 25 liter and 300 liter foam plate converter. By Michael. November 14, 1941. Frames 98-103. 5 pages.

19. State of synthetic oil experiments, February 1942. By Michael. February 13, 1942. Frames 104-105. 2 pages.

20. State of CO-H₂ synthesis in April 1941. By Michael. April 7, 1941. Frames 106-109. 4 pages.

XIII. Fuel evaluation.

1. Report on Exchange of experience on investigation of aviation gasoline. Frames 110-113

2. Knock-limit curves. Frames 114-125

3. Remarks of Fromherz on the calculation of overload curves. Frames 126-128

4. Discussion concerning quality of aviation gasoline. Frames 129-134

5. Lead susceptibility of CV2b. Frames 135-139

6. Octane number of very low endpoint gasoline. Frames 140-141

7. Knock curves of alcohol-gasoline mixtures. Frames 142-147

8. Comparison between the knock limit curves (Oppau method) with the overload curve (DVL method). Frames 148-155

10. A specification for aviation gasoline. Frames 156-157

14. Knock tests with aromatic mixtures. Frames 158-167

XIV. General.

1. Difference between various methods of “upgrading” coal (i.e. to oils of higher value). Frames 168-179

2. On destructive hydrogenation (Russian article by P. W. Putschkow). (In German). Frames 180-215

3. Theory of the ammonia catalysts. Work of the I. G. Frames 216-223

7. Bauxite residues of the Al₂O₃ preparation. Frames 224-226

8. Drying of coal in Belgium. Frames 227-228

9. Briquetting with hydrogenation residues. Frame 229

10. Avoiding employment of people with foreign affiliations. Frame 230

XV. Instrumentation.

1. Brief summary of high pressure instrumentation applications. Frames 231-232

2. Use of H and B regulators for temperature control. Frames 233-236

XVI. Liquid phase hydrogenation.

1. Decreasing the preheater load. Frames 237-239

2. Paste regeneration. Frames 240-242

3. Installing carbonization plants in connection with hydro plants. Frames 243-244

4. Adding very hot hydrogen to moderately heated paste before hydrogenation. Frames 245-247

5. Research report. Running Silesian coal K1160 to gasoline and middle oil at 600 atm. in 10 liter converter. Frames 248-273

6. On the chemical composition of preheater incrustation. Frames 274-276

7. Decreasing the liquid phase preheater load. Frames 277-287

8. Research report. Running Silesian coal K1197 to gasoline and middle oil at 600 atm. in 10 liter oven. Frames 288-379

9. Possible substitutes for NH₄Cl in hydrogenating Ruhr coal. Frames 380-382

10. Exchange of experiences on use of a fifth converter. Frames 383-385

12. Applying small scale results to hydrogenation of Upper Silesian coal at Blechhammer, Ludwigshafen, Oct. 25, 1943 Frames 386-389 .

13. Use of a tin-containing dust as catalyst. Frames 390-391

14. Occurrence of a caviar-like formation in #1 converter during the large scale work on fuel oil production with Upper Silesian coal. Frames 392-394.

15. Means of producing fuel oil. Frames 395-397

16. Research report. Running Scholven coal K1101 with chlorine added in various ways and tin oxalate to gasoline and middle oil in 10 liter converter at 250 atm. Frames 398-444

17. Research with Rhenish brown coal in one liter converter. Neutralization of coal and settling operations. Frames 445-448

18. Caviar formation. Frames 449-450

19. Autoclave work on Scholven coal. Frames 451-452

20. Autoclave work on Upper Silesian coal. Frames 453-455

21. Caviar formation from Rhenish brown coal in 10 liter converter. Frames 456-461

22. How compositions of products vary with nature of operations in bituminous coal hydrogenation. Frames 462-464

23. Comparative hydrogenability of various kinds of coal. Frames 465-467

24. Liquid phase catalysts. Frames 468-471

25. Autoclave work on Puertellan coal. Frames 472-476

26. Table. Results of large pilot plant work to produce gasoline and varying amounts of fuel oil. Frame 477

27. Autoclave work on Brux tar. Frames 478-483

28. Running bituminous coal and bituminous coal high temperature tar. Frames 484-505

29. Research report. Running Silesian coal K1174 to an excess of heavy oil at 600 atm. in 10 liter converter. Frames 506-536

31. Previous results on hydrogen with elementary sulfur on various raw materials. Frame 537.

34. H.O.L.D. filtration research with several solvent additives. Frames 538-539

35. Reports on Kipp filter research with TTH separator residue. Frames 540-559

37. Report on revolving filter research with TTH separator residue. Frames 560-571

38. Hydrogenation of old coals. Frame 572

39. TTH treatment of Deuben carbonization tar. Frames 573-578

40. Running old Gelsenberg coal (K1086) to gasoline and middle oil at 600 atm. Frames 579-593

41. Research report. Running German crude oil in 10 liter converter. Frames 594-628

42. Operation exchange of experience. Frames 629-643

43. Gasification when running Silesian bituminous coal and tar there from to heavy oil at 600 atm. Frames 644-645

44. Substituting NH4Cl in the case of Scholven coal (Autoclave work at 350 atm.) Frames 646-648

45. Fuel oil discussion (Gelsenberg 1942). Frames 649-652

46. Cold paste injection at Scholven. Frames 653-654

47. Comparison of H.O.L.D. tests. Frames 655-657

48. Fuel oil and electrode coke. Frames 658-661

49. Liquid phase treatment of H.O.L.D. at 600 atm. in 1.5 liter converter. Frames 662-665

50. Saving Mo in the liquid phase. Frames 666-66

51. Scholven coal at 600 atm. with iron catalyst and chlorine. Frames 669-671

52. Research report. Addition of Na₂S in bituminous coal hydrogenation. Frames 672-699

53. Research report. Running Silesian coal pasted with tar from Silesian coal to a low excess of heavy oil at 600 atm. in 10 liter converter. Frames 700-720

54. Table showing liquid phase. LPG distribution when running Upper Silesian coal to heavy oil excess. Frames 721-722

55. Iron-grude catalysts at various temperatures. Frames 723-725

56. Processing C-rich bituminous coal. Frame 726

57. Coal as catalyst in hydrogenation of pitch-tar mixtures (autoclave work). Frames 727-729

58. Catalyst research for pitch-tar mixture. Frames 730-731

59. Extraction of primary bitumen depending on the age of the coal. Frames 732-734

60. Coal extraction discussion at Ruhrol. Frames 735-737

61. Investigation of extraction solvent at Lutzkendorf. Frames 738-741

62. Investigation of the phenol extraction outfit at Lutzkendorf. Frames 742-771

63. Extraction research in autoclaves for production of primary bitumen. Frames 772-781

64. X-ray investigation of caviar. Frame 782

65. Filter research in 1937. Frames 783-788

66. Further results of filter research of hydrogenation residues. Frames 789-790

67. Use of hydrogenation pitch as a briquetting material for bituminous coal. Frames 791-797

68. Research report. Running bituminous coal and carbonization tar to briquetting material and asphalt free oil. Frames 798-840

69. Blechhammer briquetting research. Frames 841-842

70. Coking hydrogenation residues in mixture with coal in loose condition. Frames 843-855

110. Group analyses of Abschlamm. Frames 856-877

119. Liquid phase catalyst tests in rotating autoclaves. Frames 878-883

120. Abschlamm regenerator. Frames 884-896

XVII. Liquor treatment.

1. Research to expel phenols from waste waters of hydro plants through use of them. Frames 897-923

2. Processing residue oil from liquor treatment. Frames 924-925

3. Working of the creosote oil S obtained from the tri-cresyl-phosphate liquor process. Frames 926-938