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T.O.M. Microfilm Reel 203

(Original designation LF – 125)

Table of Contents

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Hochdruckversuche Laboratories

I.              Lectures By Dr. Pier.

II.            Reports On Experimental Work On Hydrogenation In The Sumpfphase.  Files Of Dr. Peters.

III.           Reports On Experimental Work In The Sumpf-Phase Of Dr. Peters.

Source of Documents:  Griesheim Central I.G. Library

Folder Nos.:          S33/I-C-9

                                S33/I-D-6

                                S33/I-D-7

Filmed by:              J I O A

Date:                       28 February 1946.

I.                Hochdruckversuche Laboratories.  Lectures by Dr. Pier.        S33/I-C-9.

Item

1.             Hydrogenation gasoline.  Influence of crude material, catalyst and method of processing.  Frames 1-34

2.             Competitor Michal.  Frames 35-40

3.             Hydrogenation gasoline.  Influence of crude material, catalyst and method of processing.  Frames 41-45

4.             Solid-bed catalyst and gas phase.  Frames 46-54

5.             Gas phase gasolines as dependant on the crude materials.  Frames 55-61

6.             Solid-bed catalyst and gas phase.  Frames 62-69

7.             Sumpf phase.  Frames 70-84

8.             Hydrogenation gasoline.  Influence of crude material, catalyst and method of processing.  Frames 85-100

9.             Talk on hydrogenation delivered at Rom.  Frames 101-120

10.           Hydrogenation gasoline.  Influence of crude material, catalyst and method of processing.  Frames 121-129

11.           The treatment of shale oil by hydrogenation.  Frames 130-156

12.           Draft for the talk on shale oil.  Frames 157-162

13.           Working of Scotch shale oil.  Frames 163-165

14.           Pressure hydrogenation experiments with Scotch shale oil.  Frames 166-178

15.           Lubricant from Scotch shale oil over catalysts 5058 and 6719 at different pressures.  Frames 179-184

16.           Talk on hydrogenation delivered at Glasgow.  Frames 185-193

17.           Sumpf phase.  Frames 194-202

18.           Gas phase.  Frames 203-208

19.           Requirements put to the fuels by the combustion engine and ways to their realization in Germany.  Frames 209-243

II             Hochdruckversuche Laboratories.  Reports on experimental work on hydrogenation in the Sumpfphase.  Files of Dr. Peters – S33/I-B-6.

Item

1.             Processing a pitch mixture from Welheim (P 1487 of August 18, 1941) at 600 atm to heavy oil excess in 10 litre furnace.  Frames 244-272

2.             Processing a mineral-coal-tar mixture for Politz at 600 arm to gasoline and heavy oil in 10 litre furnace.  Frames 273- 298

3.             Processing high temperature carbonization tar “Carsten Zentrum of the “Schlesag” (P 1376 from June 6, 1940) at 600 atm for excess heavy oil.  Frames 299-332

4.             Comparing the various “Sumpfphase” systems as to the heat required and to the course of temperature.  Frames 333-336

5.             Preliminary report on hydrogenation experiments with “Otto” tar and “Oheim” nutcoal.  Frames 337-338

6.             The accuracy of elementary uncorrected balances on the 10 liter furnace.  Frame 339

7.             Processing a mineral-coal-tar mixture for Politz at 600 atm for excess heavy oil in 10 liter furnace.  Frames 340-372

8.             Processing a mixture of coke oven tar (Ruhr) (P 1416) topped up to 325° at 600 atm, for excess heavy oil in the 10 liter furnace.  Frames 373-406

9.             Processing coke oven tar “Auguste Viktoria” (Ruhr) (P 1094 of July 11-39) topped up to 325° at 600 atm, for excess heavy oil in 10 liter furnace.  Frames 407-437

10.           Processing coke oven tar “Auguste Viktoria” (Ruhr) topped up to 325° (PM1094 of July 11-1939) at 600 atm, to gasoline and middle oil.  Frames 438-476

11.            Problems in processing “Rheinische Braunkohle” (soft coal).  Frames 477-478

12.            Preheater coils of 10 liter furnace becoming incrusted.  Frames 479-485

13.            Supplement: Processing of “Scholven” sludge in “Sumpf” phase at 600 atm in 1.5 liter furnace.  Frames  486-489

14.           Testing Brux embers as catalyst carriers.  Frames 490-491

15.           C-H-analyses of various products from chamber 804 Ludwigshafen charged with Upper Silesian coal for

    gasoline and middle oil (August 1941).  Frame 492

16.           Processing Scholven coal (Zweckel coal) with iron catalyst and chlorine.  Frames 493-495

17.           Applying very high thru puts in processing Silesian coal for maximal excess of heavy oil.  Frames  496-499

18.           Processing Silesian coal “K 1174” “Castellengo – Abwehr” to gasoline and middle oil at 600 atm in 10 liter furnace.  Frames 500-534

19.           Experiments in 10 liter furnace on Sumpfphase problems.  Frame 535

20.           Processing Silesian coal “K 1180” from “Beuthengrube” for gasoline and middle oil at 600 atm in 10 liter furnace.  Frames 536-582

21.           The effect of the age of coal on the quality of the fuel oil.  Frames 583-584

22.            Processing “Scholven” sludge in Sumpfphase at 600 atm in 1.5 liter furnace.  Frames 585-593

23.           Experiments in processing crude oil residue from "Heide” at 600 atm to Diesel fuel.  Frames 594-597

24.           Note re problem of conversion of Na2CO3 to Na2S when sulfurizing the “Bayermass” with pure H2S and H2S-CO mixtures.  Frame 598

25.           Re:  Hydrogenation of pitch.  Frame 599

26.           Processing Silesian Mineral coal 1160 (Preussengrube) to heavy oil excess at 600 atm in 10 liter furnace.  Frames 600-630

27.           Middle oil concentrations in the mineral coal “Sumpfphase” in different procedures of production.  Frame 631

28.           Experiments on obtaining primary bitumen for the manufacture of electrode carbon (preliminary stage).  Frames 632-635

29.           Experiments on heating coal paste.  Frames 636-653

30.           Processing Silesian coal “K 1174”. “Castellengo-Abwehr” to excess heavy oil at 600 atm in a 10 liter furnace.  Frames 654-685

31.           The influence of the content of middle oil in paste oil on the composition of the re-formed products when processing Silesian coal “K 1197” by varying procedures.  Frames 686-691

32.           Processing Silesian coal from the “Heinitz” pit to heavy oil excess under extensive decomposition of the asphalts.    Frames 692-694

33.           Processing hydrogenation residues rich in asphalts, by carbonizing them mixed with coal to a loose charge.  Frames 695-707

34.           Re: Economizing molybdenum in the Sumpfphase.  Frames 708-710

35.           Processing a mineral coal-tar mixture (Politz) in the 10 liter furnace over “Grude” iron-titanium catalyst.  Frames 711-713

36.           Composition of gases from processing Silesian mineral coal and high-temperature tar from mineral coal at 600 atm. to heavy oil.  Frames 714-715

37.            Processing “Boehlen” coal in the Sumpfphase.  Frames 716-717

38.            Experiments with mineral coal tar in the 10 liter furnace.  Frames 718-719

39.           Heating fuels from various mineral coals.  Frames 720-724

40.           Comparing the qualities of heating fuels obtained from heavy oils by various procedures.  Frames 725-727

41.           Program for a conference with Mr. Josenhans at Lu on January 15, 16 and 17, 1941.  Frames 728-729

42.           On the problem of substituting molybdenum in processing tar at Politz.  Frames 730-731

43.           Processing of mineral coal for various yields of heavy oil excess.  Frames 732-737

44.           Silesian mineral coal 1118 from the pit “Grafin Johanna” of the “Grafl. Schaffgott’schen works Ltd.”, processed for obtaining gasoline and middle oil at 600 atm. in the 10 liter furnace.  Frames 738-770

45.           “Sudenten” tar (“Lurgi” tar from Brux coal).  Frames                 771-796

46.           Chlorine contents of raw material provided for “Blechhammer” and of oils produced from these.  Frames 797-798

47.           Processing coke oven tar pitch (admixture of chlorine).  Frames 799-801

48.           Hydrogenating non-de-ashed Upper Silesian coal with chlorine.  Frames 802-806

49.           Simultaneous hydrogenation of Silesian mineral coal and low temperature carbonization tar.  Frames 807-811

50.           First figures on processing high temperature tar from carbonization of Upper Silesian mineral oil.  Frames 812-813

51.           Status of experiments with Sudenten coal at 600 atm.  Frames 814-815

52.           Status of experiments with Sudenten coal at 250 atm.  Frames 816-817

53.           Fuel oil form stripper heavy oil.  Examining stripper fractions.  Frames 818-820

54.           Stage of experiments with “Bubiag” coal (K 197) at 600 atm.  Experiments in 1.5 liter furnace with stirrer.  Frames 821-822

55.           Hydrogenation of coal tar in Sumpfphase at 600 atm. to gasoline and fuel oil.  Frames 823-832

56.           Progress in hydrogenation of open-burning coal. Experiments with “Gelsenberg” coal (83.9% C in dry coal) in the 10 liter furnace with stirrer.  Frames 833-834

III.                  Hochdruckversuche Laboratories. Reports on experimental work in the Sumpfphase.  Files of Dr. Peters.    S33/I-D-7.

Item

1.             Problems of starting (in the Sumpf” phase).  Evaluation of the 10 liter furnace experiments up to now.  Frames 835-846

2.             Processing mineral coal to gasoline, middle oil and light heavy oil.  Frames 847-848

3.             Centrifuging tars and sumpfphase sludges from tars.  Frames 849-852

4.             Sludge distillation.  Report I.  Frames 853-868

5.             Processing “Janina” coal to gasoline and middle oil at 250 atm with iron catalysts.  Frames 869-875

6.             Heating fuel from “Janina” coal.  Frame 876

7.             Processing “Janina” coal at 600 atm to excess heavy oil.  (First preliminary report.).  Frames 877-879

8.             Processing “Janina” coal at 600 atm to gasoline and middle oil.  (Second preliminary report.).  Frames 880-887

9.             Relation between analyses of coal and behavior in hydrogenation.  Frames 888-890

10.          On pre-heating cracking residues.  Frames 891-896

11.          The question of incubation temperature.  Frames 897-898

12.           Measuring the heat transfer from mineral coal paste.  Frame 899

13.           Hydrogenation of “Janina” coal to gasoline and middle oil at 600 atm.  First results.  Frames 900-904

14.           Status of experiments on the 10 liter furnace.    Frame 905

15.           Processing petroleum in straight passage.  Frames 906-907

16.           Experiments in 1-liter furnace with sulfur as “Sumpfphase” catalyst.  Frames 908-913

17.           “Starting” in coal hydrogenation in the Sumpfphase.  Frames 914-916

18.           Processing “Myslowitz” coal at 600 atm to gasoline and middle oil.  Frames 917-918

19.           Producing slightly hydrogenated coal from K 1197 at 300 atm.  Frames 918-928

20.           Comparing sodium sulfide raw smelting with Sulfigran.  Frames 929-930

21.           Catalyst experiments in 1.5 liter furnace for processing “Bruex” tar.  Frames 931-936

22.           Admixture of sodium-sulfide in mineral coal hydrogenation.  Older experiments with K 1090 (Gelsenberg) in 10-liter furnace.  Frames 937-964

23.           Processing mineral coal together with mineral coal extract.  Frames 965-966

24.           Processing mineral coal high temperature tar with mineral coal admixed.  Frames 967-989

25.           Processing mixtures of “Bohlen” tar and petroleum (August 1939).  Frames 990-1007

26.           Report on experiments:  Processing of Panuco-oil in 10 liter furnace.  Frames 1008-1028

27.           Processing “Bohlen” tar at 250 atm. in 10 liter furnace.  (August 1939).  Frames 1029-1043

28.           Report on experiments: Processing German petroleum in 10 liter furnace.  Frames 1044-1077

29.           Processing mineral coal and carbonization tar to briquette binder and asphalt-free oil.  Frames 1078-1121

30.           Processing “Zweckelcoal” (K 1216) to gasoline and middle oil at 600 and 250 atm and to heavy oil excess at 600 atm in 10 liter furnace.  Experimental report.  Frames 1122-1163

31.           Extractive hydrogenation of mineral coal.  Frames 1164-1231

32.           Processing Silesian coal (K 1197) together with Silesian mineral coal-tar mixture to a slight heavy oil excess at 600 atm in the 10 liter furnace.  Frames 1232-1254

33.           On “caviar” formation”  Experiments with “Rhine” soft coal in 10 liter furnace.  Frames 1255-1260

34.           Experimental report:  Processing a mixture of Silesian mineral coal tars at 600 atm to heavy oil excess in the 10 liter furnace.  Frames 1261-1283

35.           First figures on processing primary bitumen by hydrogenation.   Frames 1284-1286

36.           Re: Processing hydrogenation coal “Scholven” K 1101 of September 30, 1938, at 250 atm with chlorine, in various forms of admixture and with “Snox” for obtaining gasoline and middle oil.  Report on experiments in the 10 liter furnace.  Frames 1287-1330

37.           Extractive hydrogenation in 10 liter furnace.  Frames 1331-1335

38.           Preventing crusts and blockings of coal furnaces at Scholven.  Frame 1336

39.           Experiments on “Caviar” formation in the rotary autoclave.  Frames 1337-1338

40.           Experiments with Rhine brown coal in 1 liter furnace.  Note No. 3:  Neutralization of coal and its tendency to deposit.  Frames 1339-1340

41.           Joint processing of upper Silesian coal and rinsing gas tar to briquette binding agents and to heating fuel.  Frames 1341-1345

42.           Experimental report: Joint processing of Silesian coal (K 1197) and high temperature carbonization tar  from Silesian coal (P 1376) for obtaining slight excess heavy oil at 600 atm in 10 liter furnace.  Frames 1346-1373

43.           The status of experiments with Rhine brown coal.  Frames 1374-1375

44.           Experiments with Rhine brown coal in 1 liter furnace.  Preliminary notes on “caviar” formation.  Frame 1376

45.           Supplement to report 20 4721 of July 16-42:  Preliminary report on hydrogenation experiments with B.T. – tar from “Oheim” nut coal.  Frame 1377