T.O.M. Microfilm Reel 201
(Original designation LF 99)
Table of Contents
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Hochdruckversuche Laboratories - File of Dr. Simon. Papers on Hydrogenation, Aromatization, and Paraffin Oxidation.
Source of documents L. Griesheim Central I. G. Library.
Folder No. S-32/VIII-D-2
S-32/VII-D-1
S-32/VII-D-6
S-29/X-D-3
Filmed by: JIOA
Date: 28.1.46
Section I. Papers on Hydrogenation
Item
1. Influence of the temperature on the reactions taking place during the hydrogenation of bituminous coal liquefaction middle oil over catalysts 5058, 7846, and 8376. Frames 1-20
2. Contribution to the theory of sumpf phase. Frames 22-24
3. Benzination of DHD-residue. Frame 25
4. Experiments concerned with the testing of the motor behavior of auto hydrogenated polymer gasoline. Frames 26-28
5. Report on activities, October 1943. Frames 29-35
6. Pressure refining of sumpf gasoline at different temperatures. Frames 36-39
7. Experiments on the isomerization n-heptane from normal heptane by means of catalysts 5058 in the rotary autoclave. Frames 40-41
8. Gas phase catalysts. Frames 42-43
9. Recent investigations into the field of benzination catalysts. Frames 44-48
10. Concerns: Back flow due to the collapse of a high pressure pipe line. Frames 49-51
11. The influence of the products partial pressure on the aromatization of bituminous coal liquefaction middle oil Scholven over alumina-Terrana catalyst 8688. Frames 52-56
12. The influence of the nitrogen contents of oils on their capability to be benzinated. Frames 57-64
13. Removal of the heat of reaction in gas phase hydrogenation by pumping the circulating gas while hot. Frames 65-67
14. The testing of regenerated 6434 catalysts. Frames 68-69
15. Experimental basis for the working of heavy oils with solid catalysts. Frame 70
16. The influence of sulfur addition on the 250 atms. Aromatization of bituminous coal liquefaction middle oil with alumina Terrana catalyst. Frame 71
17. The influence of adding organic nitrogen compounds on the results of benzination of crude oil-gas oil over catalyst 6434. Frames 72-76
18. The effects of W, Ni, Co and Fe as active components on alumina pre-hydrogenation catalysts. Frames 77-85
19. Our supply of liquid fuels. Frames 86-104
20. The mechanism of hydrogenation – catalysis. Frames 105-108
21. Gasoline from bituminous coal via fuel oil – Diesel oil. Estimate. Frames 109-110
22. Decreasing and increasing temperature during the hydrogenation of Upper Silesian bituminous coal. Frames 111-112
23. Centrifugal experiments with sludge from the tar chamber Brux. Frames 113-114
24. The action of sodium sulfide on stripper heavy oil. Frames 115-116
25. New benzination catalysts. Benzination catalysts free from tungsten of the oxide-fluoride of Si, Al, and Fe type. Frames 117-121
26. Benzination of P 1203/8376 B-M’ oil over 6434 & 8797. Frames 121-127
27. Contribution to the theory of ash-balance. Frames 128-131
28. Ash balances of autoclave experiments with bituminous coals. Frames 132-140
29. The heating up of cracking residues. Frames 141-143
30. Replacement of ammonium chloride with Scholven coal. Frames 144-146
31. Analysis of low temperature carbonization residue from shale for their possible use as sumpf phase catalysts. Frames 147-150
32. Older hydrogenation experiments with arsenic compounds. Frames 151-153
33. Starting of coal hydrogenation in the Sumpf phase. Frames 154-156
34. Measurements concerning heat transfer in bituminous coal paste. Frames 157-158
35. About the question of the starting temperature. Frames 159-160
36. Influence of the nitrogen content on the capability of oils to be benzinated. Frames 161-163
37. Note on the production of iso-heptane from normal heptane at 50 atms. over catalyst 5058 with hydrochloric acid addition. Frame 164
38. Isomerization of hydrocarbons. Frames 165-168
39. The butane and iso-butane contents in the gases from benzination and aromatization with bleaching earth catalysts. Frames 169-170
40. Working of bituminous coal liquefaction middle oil over pre-hydrogenation/7846 W 250, benzination and DHD. Frames 171-188
41. The influence of temperature on the results of the prehydrogenation with concentrated and diluted catalysts. Frames 189-190
42. Dehydrogenation and refining of polymer gasoline. Frames 191-193
43. Influence of the addition of organic nitrogen compounds on the results of the benzination of crude oil gas over catalyst 6434 II. Frames 194-196
44. Requirements in rare metals in the gaseous phase with these production methods for gasoline which are most important at the present time. Frames 197-204
45. Influence of the re-cycle ration on the 250 at aromatization of bituminous coal liquefaction middle oil over alumina-Terrana catalyst 8688. Frames 205-213
46. The dependence of knocking properties of gasoline and gasoline fractions on the starting material. Frames 214-222
47. The behavior of acid and basic components of bituminous coal liquefaction middle oil during the prehydrogenation with alumina catalysts. Frames 223-227
48. Working of vacuum distillate from a stripper heavy oil at 600 atm. over solid-bed catalyst for Diesel oil with low pour point. Frames 228-232
49. Splitting of heavy stripper oil from bituminous coal over solid-bed catalyst at 250 and 600 atm. Frames 233-244
50. Calculations bearing on the question 300 vs. 700 atm. Frames 245-247
51. Improvement of the low temperature carbonization yield in the separator. Frames 249
52. Testing of some new pre-hydrogenation catalysts. Frame 250
53. Prehydrogenation of P 1271 with catalyst 8807/8376 and 8806/8376. Frames 251-253
54. Laboratory and industrial experiments aiming at increase in the yield in low temperature carbonization of asphalt containing residues. Frames 254-257
55. Relations between coal analyses and behavior during hydrogenation. Frames 258-262
56. The influence of the sulfur addition on the benzination over catalysts 6434. Frames 263-265
57. Crystallographic report on ammonium sulfotungstate. Frames 266-268
58. Experiments in the 1 ltr. Furnace with sulfur as Sumpf phase catalyst. Frames 269-274
59. Notes on the splitting effect of WS. Frame 275
60. Possible replacement of ammonium chloride in the hydrogenation of Ruhr coal. Frames 276-278
61. Influence of the size and density of the catalyst pills on the benzination and prehydrogenation with catalyst 5058. Frames 279-289
62. Filtration of sludge with the addition of higher alcohols from the iso-butylalcohol production. Frames 290-291
63. Autoclave experiments aiming at the splitting of paraffins with tungsten sulfide by means of hydrogenation. Frames 292-310
64. New results concerning the lattice disturbance of the active tungsten sulfide. Frames 311-315
65. Experimental results with tungsten catalysts. Frames 316-319
66. Tungsten oxides. Frames 320-325
67. Research into the principles of catalysis. Frames 326-327
68. Addition of sodium sulfide in the hydrogenation of bituminous coal. Frames 328-355
69. Sulfur absorption of the unsulfurated Bayer mass under high pressure. Frames 356-358
70. Sensitivity to nitrogen and other disturbance. A comparison between catalysts 8797 and 6434. Frame 359
71. Extended prehydrogenation tests of bituminous and brown coal liquefaction middle products over catalysts 8376 – 7846 W. 250 without sulfur addition to the products. Frames 360-367
72. New benzination catalysts. Frames 368-381
73. Catalysts 5058 in combination with catalyst 7846. Frames 382-384
74. Experiments in the 1 ltr. Furnace aiming at the splitting of stripper heavy from bituminous coal at 250 atm. with solid-bed, regenerable catalyst. Frames 385-398
75. Determination of aromatics in gasoline by light absorption measurements. Frames 399-400
76. Production of gasoline from petroleum or propane de-asphalted and de-waxed vacuum residue from German crude oil. Frames 401-403
77. Hydrogenation of ld aviation lubricant. (1580) Frames 404-409
Section II
1. Conference with OHW at Ludwigshafen on the 25th of October 1943. Subject: Results obtained with small scale apparatus. Frames 410-413
2. Directions for the mode of construction of high pressure hydrogenation chambers. Frames 414-415
3. Exchange of experience: Sieve analysis of coal and coal paste. Frames 416-417
4. Electric pre-heaters, Chamber 2. Frames 418-423
5. Exchange of experience: electric pre-heaters. Frames 424-427
6. Exchange of experience: electric pre-heaters. Frames 428-429
7. Questionnaire for collecting the data necessary for calculating gas hydrogenation products. Frames 430-454
8. Exchange of experience of Dec. 4, 1941, at Ludwigshafen. Frames 455-470
9. Comparison of the working conditions of some hydrogenation plants. Frame 471
10. Basic data for the hydrogenation of various crude materials. Frames 472-474
11. Calculation of the amount of hy-gas which is likely to accrue in the bituminous coal hydrogenation “Hibernia”. Frames 475-532
12. Fuel oil conference at Scholven on 5 Jan. 1942. Frames 533-535
13. Fuel oil conference at Gelsenberg on 5 Jan. 1942. Frames 536-539
14. Regeneration of bituminous coal paste. Frames 540-542
15. Increasing the low temperatures carbonization yield by addition of catalysts and surplus steam. Frames 543-549
16. Report on a conference held at the premises of Mineralol-Baugesellschaft Limited Co., Berlin, on the 14th, 2, 1941. Subject: Coal preparation plants. Frames 550-554
17. Conference at Scholven. Frames 555-560
18. Heating up by means of super-heated hydrogen. Frames 561-563
19. Relief of the Sumpf phase pre-heaters. Frames 564-575
20. The chemical composition of the crusts formed in the pre-heaters. Frames 576-578
21. Velocities in the high pressure furnaces. Frames 579-581
22. The gas circulation in 700 atm hydrogenation chambers, particularly from a point of view of measuring technique. Frames 582-588
23. What is to be found in the literature on gas hydrogenation products. Frames 589-597
24. Exchange of experience: gas hydrogenation products. Frames 598-611
25. High pressure experiments. Frames 612-613
26. Hydrogen partial pressure in the 7019 gas circulation. Frames 614-623
27. Comparison of the costs of 7019, 5058 and 6434 chambers. Frames 624-630
28. Solubility of the hydrogenation components in the Sumpf phase in the bituminous coal hydrogenation at 700 and 300 atms. Frames 631-635
29. Possibility for the production of phenol in the hydrogenation of coal. Frames 636-637
Section III
1. Polycyclic aromatics from hydrogenation products. Frames 638-653
2. Coronen. Frames 654-673
3. Aromatization of bituminous coal liquefaction middle oil Scholven P 1271 at 600 atm. Over the new Welheim catalyst (Lu Nr. 8213) produced at Ludwigshafen. Frames 674-679
4. Notes on aromatization at 250 and 600 atms. Frames 680-687
5. Behavior or aromatic and aromatic gasolines on the addition of lead tetra ethyl. Frames 688-692
Section IV
1 Hydrogenation and low temperature carbonization in the field of synthetic motor fuel production. Frames 693-700
2. The present status of the low temperature bituminous coal carbonization and plans for enlargement of the GB Chemie. Frames 701-730
Section V