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T.O.M. Microfilm Reel 166

 

(Original Designation LF-68)

 

Table of Contents

 

Note from the editors – only selected documents from this microfilm reel have been completely processed and presented below in cleaned and grouped format (Section IV, items 5-7, Section V item 1 and 3, Section VI item 2, and Sections VII and VII, all items, identified by HTML links below.  The remainder of the reel is not related to the Fischer-Tropsch process, and therefore complete processing cannot be justified at this time.

 

We are, however, making the entire reel contents available in raw image format, although in a small number of relatively large files (rather than a very large number of small individual images).  Anyone interested in pursuing the non-FT related material on this reel may find the document in these larger raw files. 

 

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I.              Drawings For Experimental Hydrogenation Equipment.

II.            Hochdruckversuche Laboratories.  Experimental Coal Hydrogenation In 10-Ltr. Furnaces.

III.           Hochdruckversuche Laboratories.  Miscellaneous Papers On Aromatization.

IV.           Hochdruckversuche Laboratories.  Work On Lubricating Oils.

V.            Hochdruckversuche Laboratories.  Reports On CO-H2 (Fischer-Tropsch) Synthesis.

VI.           Hydrierwerk Scholven.  Papers Concerned With Desulphurization By F-Coal.

VII.         Hochdruckversuche Laboratories.  Reports On Michael (Fischer-Tropsch) Hydrocarbon Synthesis.

VIII.        Hochdruckversuche Laboratories.  Reports On (Fischer-Tropsch) Hydrocarbon Synthesis.

 

 

Source of Documents:                             Griesheim Central I. G. Library

Folder Nos:                                             S28/III-A-8             S29/IX-C-7

                                                                S28/III-A-7             S29/IX-A-8

                            S29/III-E-11            S29/IX-C-6

                            S28/III-A-11           S29/IX-C-8

Filmed by:                                                JIOA

Date:

 

 

I.                     Drawings for experimental hydrogenation equipment.  Folder No. S28/III-A-8.  Frames 1-118

 

II.                   Hochdruckversuche Laboratories.  Experimental coal hydrogenation in 10-ltr. furnaces.  Folder No. S28/III-A-7.

 

1.             Extractive hydrogenation of bituminous coal.  Frames 119-186

 

2.             Combined working of Silesian coal (K 1197) and high temperature carbonization tar from Silesian coal ( 1376) for a small excess in heavy oil at 600 atm in the 10 liter. furnace.  Frames 187-214

 

3.             Working of high temperature carbonization tar “Gartsten – Zentrum” of the “Schlesag” at 600 atm. for an excess in heavy oil.              Frames 215-250

 

4.             Working of a bituminous coal tar mixture for Politz at 600 atm for an excess in heavy oil in the 10 liter furnace.  Frames 251-285

 

5.             Working of a mixture of carbonization tars (Ruhr) at 600 atm. for excess in heavy oil in the 10 liter furnace.  Frames                          284-317

 

6.             Working of carbonization tar “Auguste   Viktoria” (Ruhr) at 600 atm. for an excess in heavy oil in the 10 liter furnace.  Frames  318-348

 

III.                 Hochdruckversuche Laboratories: Miscellaneous papers on aromatization. Folder No. S29/III-E-11.

 

1.             The influence of the product partial pressure on the aromatization of bituminous coal liquefaction middle oil Scholven over alumina-Terrana catalyst 8688.  Frames 349-355

 

2.             Influence of  catalyst, pressure and product partial pressure on cracking and hydrogenation of Bruchsal gas oil.  Frames    354-362

 

3.             Aromatization at 250 atm. with alumina-Terrana catalyst of the type 8688.  Frames 363-374

 

4.             Influence of the re-cycle ratio on the 250 atm. aromatization of bituminous coal liquefaction middle oil over alumina-Terrana contact 8688.  Frames 375-382

 

5.             Influence of the though-put on the 250 atm. aromatization of bituminous coal liquefaction middle oil over alumina-Terrana catalyst.  Frames 383-389

 

6.             The influence of pressure on the aromatization of bituminous coal liquefaction middle oil with Terrana catalyst.  Frames 390-397

 

7.             Aromatization at 250 atm. with alumina-Terrana catalyst 8688.  Frames 398-405

 

8.             250 atm. aromatization catalyst 8688.  Frames 406-408

 

9.             Experiments concerning aromatization at atmospheric pressure of pure n-heptane and paraffin-containing heavy gasoline.  Frames 409-411

 

10.           Catalytic experiments concerning the 250 and 600 atm aromatization in 1 liter furnaces with alumina, bleaching earth and synthetic silicate catalysts.  Frames 412-427

 

11.           Testing of aromatization catalyst at 250 atm in 100 com lead bath furnaces.  Frames 428-441

 

12.           Amount of gasification and composition of the gases in the aromatization of bituminous cool liquefaction middle oil, as dependant on the catalyst used and the experimental conditions.  Frames 442-452

 

13.           Reason for differences in quality between rest gasolines from the aromatization of bituminous coal liquefaction.  Frames 453-462

 

14.           Aromatization experiment over catalyst 7019 with subsequent alumina catalyst.      Frames 463-468

 

15.           Aromatization at 250 atm over alumina catalyst.       Frames 469-492

 

16.           Dehydrogenation experiments for testing aromatization catalysts.  Second continuation.  Frames 493-517

 

17.           Dehydrogenation experiments for testing aromatization catalysts.  First continuation.  Frames 518-539

 

18.           Aromatization experiments.  Frames 540-549

 

19.           7019 catalysts.  Preparation of the carrier.  Frames 550-554

 

 

IV.                Hochdruckversuche Laboratories:  Work on Lubricating oils.  Folder No. S28/III-A-11.

 

1.             Experiments aiming at the improvement of lubricants with catalyst 8376 in the 1 liter furnace.  2.  Experiments with           propane refining products from Lutzkendorf heavy oil. Comparison with catalyst K 7846.               Frames 555-567

 

2.             Hydrogenation of old  aviation motor oil (P 1580).  Frames 568-573

               

3.             Experiments aiming at the improvement of lubricants with     catalyst 8376 in the 1 liter furnace.  Comparison with             catalyst 5058.  Frames 574-586

               

4.             Tests on models concerning dilution of lubricants.  Frames 587-607

 

5.             Refining of TTH paraffin of the Brabag-Zeitz Works at 300 atm. over catalyst 8376 in chamber 501/502.  Frames 608-616.  13 pages.  Text extremely poor, tables and figures generally better.

 

6.             Splitting of paraffins of high molecular weight which have been obtained by Fischer’s synthesis.  Catalysts used for          splitting process: 5058 and 8376.  Pressure: 250 atm.   By Peters, et al.  Frames 617-620.  5 pages.

                                               

7.             Hydrogenation processing of special hard waxes obtained by the Fischer synthesis over catalysts 8376 at 250 atm.  By Peters, et al.  April 1943.  Frames 621-640.  24 pages.

                               

 

V.                  Hochdruckversuche Laboratories Reports on CO-H2 synthesis.  Folder No. S29/IX-C-7.

 

1.             Cost estimate of Michael-synthesis of olefins in the emulsion phase.  August 11, 1942.  Frames 641-645.  6 pages.

 

2.             Conference regarding OXO on September 15, 1941.  Frames 646-651

 

3.             The synthesis of olefins over Cobalt catalyst.  Frames 652-657.  7 pages.

 

 

VI.                Hydrierwerk Scholven.  Papers concerned with desulphurization by F-coal. Folder No. S29/IX-A-8.

 

1.             Sulfur-purification with F-coal.  Frames 658-665

 

2.             Report on the Ludwigshafen desulphurization plant using F-coal.  May 2, 1939.  Frames 666-674.  10 pages.

 

VII.              Hochdruckversuche Laboratories  Reports on Michael Hydrocarbon synthesis.  Folder No. S29/IX-C-6.

 

1.             Comparative analysis of the products of the gas and emulsion phase synthesis at different temperatures.  August 27, 1941.  Frames 675-685.  12 pages. 

 

2.             Deposition of the finely divided catalyst at the wall of the furnace in the emulsion method (Fischer-Tropsch hydrocarbon synthesis).  January 5, 1944.  Frames 686-694.  10 pages.

 

3.             (Fischer-Tropsch) Syntheses in the liquid phase.  Frames 695-700.  6 pages.

 

4.             Working Michael product for alcohol.  Frames 701-704.  6 pages.

 

VIII.            Hochdruckversuche Laboratories:  Reports on (Fischer-Tropsch) hydrocarbon synthesis.  Folder No. S29/IX-C-8.

 

1.             Alcohol synthesis from CO-H2 mixtures by means of the emulsion process.  By Michael.  September 13, 1941.  Frames 705-708.  5 pages.

 

2.             Alcohol synthesis from CO-H2 mixtures by means of the gas recycle process.  By Michael.  September 13, 1941.  Frames 709-712.  5 pages.

 

3.             Synthesis plant - Ludwigshafen.  April 25, 1941.  Frames 713-726.  21 pages.

 

4.             75,600 Nm3 CO plus H2 100% per hour according to Winkler from Upper Silesian bituminous coal or Leuna brown coal and low carbonization coke in the Demag generator.  May 30, 1940.  Frames 727-738.  14 pages.

 

5.             Paraffin synthesis - Dr. Michael.  May 29, 1940.  Frames 739-754.  16 pages.

 

6.             Summary of the plant estimate for the production of 100,000 t per year, using middle oil in the “Synthesis Process” (Dr. Michael).  May 6, 1940.  Frames 755-759.  5 pages.

 

7.             Personnel requirements for a plant producing 100,000 t per year, operating with middle oil, according to the “Synthesis Process” (Dr. Michael).  May 7, 1940.  Frames 760-761.  3 pages.

 

8.             Estimate of plant for the working of 100,000 Nm3 /hr ideal synthesis gas (CO plus H2) according to the Duftschmid Process.  January 12, 1939.  Frames 762-768.  8 pages.

 

9.             Comparison of the Fischer (-Tropsch) process with that of Dr. Michael.  January 1939.  Frames 769-778.  12 pages.

 

10.           Concerns:  Estimates for the I.G. Oppau plant. Oil synthesis equipment.  November 2, 1938.  Frames 779-787. 

 

11.           Working products of the synthesis for washing agents.  By Michael.  January 1942.  Frames 788-791.  4 pages.

 

12.           Syntheses experiments at 200°.  By Schmidt.  April 29, 1941.  Frames 792-794.  5 pages.

 

13.           Products obtained by the emulsion (slurry phase) operation method.  March 12, 1941.  Frames 795-797.  4 pages.

 

14.           Emulsion operation method of the hydrocarbon synthesis.  By Michael.  February 1943.  Frames 798-800.  4 pages.

 

15.           Disturbances occurring in the hydrocarbon synthesis and their prevention.  By Michael and Ehrmann.  February 18, 1943.  Frames 801-804.  5 pages.

 

16.           Alkali washing of the furnace sediment in the hydrocarbon synthesis aiming at increasing the yield of middle oil.  By Michael and Schmidt.  January 20, 1943.  Frames 805-807.  4 pages.

 

17.           Deposition of catalyst on the wall of the furnace in the emulsion (slurry phase) process.  By Michael.  November 28, 1942.  Frames 808-813.  7 pages.

 

18.           Working the products of the synthesis for alcohols, fatty acids and sulfonates.  By Michael.  June 19, 1942.  Frames 814-815.  3 pages.

 

19.           Raffination of Michael middle oil and gasoline by extraction with 70% sulfuric acid.  June 5, 1942.  Frames 816-817.  3 pages.

 

20.           The present status of the hydrocarbon synthesis by the emulsion (slurry phase) operation method.  By Michael.  May 18, 1942.  Frames 818-824.  8 pages.

 

21.           Comparative analysis of the products from the gas and emulsion (slurry) phase synthesis at different temperatures.  Frames 825-836.  13 pages.

 

22.           Carbon monoxide-hydrogen syntheses – meeting report.  By Peters.  July 23, 1941.  Frames 837-849.  16 pages.

 

23.           The present status of the hydrocarbon synthesis from carbon monoxide-hydrogen mixtures.  By Michael.  July 24, 1941.  Frames 851-861.  12 pages.

 

24.           Gasoline synthesis from carbon monoxide and hydrogen according to the gas recycle process by means of iron catalyst.      February 1941.  Frames 862-868.  8 pages.

 

 

End of Reel 166.