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Carbon Coated (Carbonous) Catalyst in Ebullated Bed Reactor For Production of Oxygenated Chemicals from Syngas/CO2:
First Annual Report for October 1, 1999 - September 30, 2000

Donald Krastman
Richard Noceti
Cynthia Mitchell

Hydrocarbon Technologies, Inc.

In this pdf format, this document has 17 pages and is 37.3KB

Table of Contents

INTRODUCTION 1
OBJECTIVE 1
WORK ACCOMPLISHED IN THE FIRST YEAR OF THE PROGRAM 2

1)

EXPERIMENTAL  
  Carbon Coating Agent 3
Extruder 3
Carbonous Extrusion and Carbon Coating 3
Carbon Coating of Extrudates 4
Preparation of Zinc-chromite Catalyst Powder 4
Cesium Doping of Zinc-chromite Extrudates 4
Preparation of K and Mn promoted ZrO2 Catalyst Powder 5
Cold-Flow Ebullated Bed Reactor 5

2)

RESULTS  
  Carbon Coating of Catalyst Extrudates Using PP Furfuryl Alcohol 5
Carbon Coating Using F-T Wax 6
Carbon Coating Using Coal Liquid 6
Carbonous Extrusion of Alumina Powder 7
Preparation of Zinc-chromite Catalyst Powder 7
Carbonous Extrusion and Carbon-Coating of Commercial Zinc-Chromite Catalyst Powder 8
Carbonous Extrusion and Carbon-Coating of Synthesized Zinc-Chromite Catalyst Powder 9
Cold-Flow Ebullated Bed Testing of Carbon-Coated Zinc-Chromite Extrudates 9
Drum Attrition Loss Test 10
Preparation of K and Mn Promoted ZrO2 Catalyst Powder 10
Carbonous Extrusion and Carbon Coating of K and Mn Promoted ZrO2 Catalyst Powder 11
Preparation for an Experimental Run Under Task III (Activity Testing) 12
Characterization of Carbon-Coated Iron Catalyst by XPS Analysis 13

3)

CONCLUSION 14