| I |
Abstract |
1 |
| II |
Objective and Scope
of Work |
3 |
| III |
Summary of Progress |
4 |
| IV |
Detailed Description
of Technical Progress |
9 |
| |
Task 1 |
Project Work
Plan |
9 |
| Task 2 |
Slurry Catalyst
Improvement |
9 |
| |
2.1 |
Wax Analysis Results |
9 |
|
2.2 |
Fixed Bed Catalyst
Studies |
11 |
| |
2.2.1 |
Run FB-99-1348 (Ruhrchemie LP 33/81) |
11 |
| 2.2.2 |
Run FA-76-0968 (100 Fe/5 Cu/4.2K/20 Al2O3) |
13 |
| 2.2.3 |
Run FA-31-1118 (100 Fe/5 Cu/4.2K) |
14 |
| 2.2.4 |
Discussion of Binder/Support Catalysts |
15 |
| 2.3 |
Catalyst Preparation and
Characterization |
14 |
| |
2.3.1 |
Catalyst Resyntheses |
19 |
|
2.3.2 |
Metal Exposure and Phase Identity
Determinations |
20 |
| 2.3.3 |
Reduction Behavior of Ruhrchemie
Catalyst |
21 |
| 2.3.4 |
Spectroscopic Studies of Catalyst
Reduction and Re-oxdation |
22 |
| Task 3 |
Process Evaluation Research |
25 |
| |
3.1 |
Slurry Reactor Catalyst Study |
25 |
| |
3.1.1 |
Run SA-99-0888 (Ruhrchemie LP 33/81) |
25 |
| 3.2 |
Slurry Reactor Catalyst Study |
25 |
| |
3.2.1 |
Run FA-63-1308 (100 Fe/5 Cu/4.2K/8 SiO2) |
28 |
| 3.2.2 |
Run FA-15-1698/FA-15-1768 (100 Fe/1.0 Cu/0.2
Cu) |
30 |
| 3.2.3 |
Run FB-99-1588 (Ruhrchemie LP 33-81) |
31 |
| V |
Literature References |
34 |
|
Tables |
35 |
| Figures |
55 |
